烧结温度对印尼当地砂合成压电用纳米二氧化硅颗粒物理、力学和电学性能的影响

IF 2.2 4区 材料科学 Q2 MATERIALS SCIENCE, CERAMICS Journal of Asian Ceramic Societies Pub Date : 2023-01-02 DOI:10.1080/21870764.2023.2173851
Muh. Sadat Hamzah, M. W. Wildan, Kusmono, E. Suharyadi
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引用次数: 3

摘要

本研究旨在确定烧结温度对纳米二氧化硅的物理、机械、介电和输出电压性能的影响。本实验中使用的纳米二氧化硅颗粒是由天然砂采用碱性熔融法制备的。在75 MPa的压力下单轴成形绿体,然后在1330、1360、1390、1420、1450℃的不同温度下在空气中无压烧结2小时。烧结结果表明,在烧结温度为1390℃时,其堆积密度最高,相对密度为2.49±0.03 g/cm3,相对密度为94.03±0.01%。烧结后二氧化硅的XRD谱图显示为石英、钇铝石和方石英相,其中最强峰对应方石英相。1390℃烧结试样的抗压强度和直径抗拉强度分别为17.23±0.27 MPa和6.06±0.71 MPa。而在烧结温度为1330℃时,其介电常数为544.28,介电损耗为195.94,输出电压为1.58 mV。不同的烧结温度对烧结试样的介电特性和输出电压没有显著影响。
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Effect of sintering temperature on physical, mechanical, and electrical properties of nano silica particles synthesized from Indonesia local sand for piezoelectric application
ABSTRACT This study aims to determine the effect of the sintering temperature of nanosilica on physical, mechanical, dielectric, and output voltage properties. The nanosilica particles used in this experiment were produced using the alkaline fusion method from natural sand. The green bodies were uniaxially formed with a pressure of 75 MPa and then were pressureless sintered at various temperatures of 1330, 1360, 1390, 1420, and 1450°C for 2 hours in an air atmosphere. The results of sintering showed that the highest bulk density and the relative density of 2.49 ± 0.03 g/cm3 and 94.03 ± 0.01% respectively were achieved at a sintering temperature of 1390°C. The XRD patterns of the sintered silica indicated phases of quartz, tridymite, and cristobalite, with the strongest peak corresponding to the cristobalite phase. The highest compressive strength and diametral tensile strength values of 17.23 ± 0.27 MPa and 6.06 ± 0.71 MPa respectively were obtained on specimens sintered at 1390°C. However, the highest values of the dielectric constant of 544.28, dielectric loss of 195.94, and output voltage of 1.58 mV were obtained at a sintering temperature of 1330°C. Various sintering temperatures do not significantly influence the characteristic of dielectric and output voltage of the sintered specimens.
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来源期刊
Journal of Asian Ceramic Societies
Journal of Asian Ceramic Societies Materials Science-Ceramics and Composites
CiteScore
5.00
自引率
4.30%
发文量
78
审稿时长
10 weeks
期刊介绍: The Journal of Asian Ceramic Societies is an open access journal publishing papers documenting original research and reviews covering all aspects of science and technology of Ceramics, Glasses, Composites, and related materials. These papers include experimental and theoretical aspects emphasizing basic science, processing, microstructure, characteristics, and functionality of ceramic materials. The journal publishes high quality full papers, letters for rapid publication, and in-depth review articles. All papers are subjected to a fair peer-review process.
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