炭黑N990作为天然碳组分的使用试验:动态特性、热稳定性和热压

Purwantiningsih Sugita
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引用次数: 0

摘要

用天然橡胶(NR)制造减振材料需要提高动态性能、热稳定性和耐热性。在NR硫化胶中使用炭黑N990作为填料可能会提高这些性能。本研究旨在研究炭黑N990对NR硫化胶动态性能、热稳定性和耐热老化性能的影响。用橡胶过程分析仪(RPA)测定了NR硫化胶的动态性能,用热重分析仪(TGA)研究了其热稳定性,并通过热老化试验测定了其耐热性。RPA测试结果表明,在NR复合材料中加入50phr炭黑N990可以将复合剪切模量提高到65%。此外,TGA测试结果表明,未填充NR硫化胶的热稳定性优于含有炭黑N990的NR硫化胶。未填充的NR硫化胶在高达353℃时热稳定,而分别含有15、30和50份/100橡胶(phr)炭黑N990的NR硫化料在高达348.1℃、348℃和349℃时热稳定性。根据ISO 4632-1的要求,结果表明含炭黑N990的NR复合材料具有良好的耐热性能。NR复合配方含有30phr炭黑N990,根据EN 15129要求显示出良好的动态性能和耐热性,因此它有潜力用作抗震结构的减振材料。
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Kajian Penggunaan Carbon Black N990 sebagai Bahan Pengisi Kompon Karet Alam: Sifat Dinamik, Kestabilan Termal, dan Ketahanan Panas
The manufacture of vibration damping material from natural rubber (NR) required an increase in dynamic properties, thermal stability, and resistance to heat. Using the Carbon Black N990 as a filler in NR vulcanizates can potentially increase on these properties. This research aims to study the effect of using Carbon Black N990 on dynamic properties, thermal stability, and aging resistance to heat in NR vulcanizates. The dynamic properties of NR vulcanizates were determined by Rubber Process Analyzer (RPA), while the thermal stability properties were studied by TGA, and heat resistance was determined by the thermal aging test. The RPA test results showed that adding 50 phr Carbon Black N990 in the NR compound could increase the value of the complex shear modulus to 65%. Furthermore, the results of the TGA test showed that the thermal stability properties of unfilled NR vulcanizates were better than that of NR vulcanizates containing Carbon Black N990. Unfilled NR vulcanizates were heat stable up to 353oC, while NR vulcanizates containing 15, 30, and 50 parts per hundred rubber (phr) Carbon Black N990, respectively, were heat stable up to 348.1oC, 348oC, and 349oC. Based on the requirements of ISO 4632-1, it showed that the NR compound containing Carbon Black N990 has good heat resistance properties. The NR compound formula contains 30 phr Carbon Black N990 showing good dynamic properties and heat resistance in accordance with EN 15129 requirements so that it has the potential to be used as a vibration damping material for earthquake-resistant structures.
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