开孔镍基金属玻璃晶格结构(Ni60Nb20Ta20)的激光增材制造与表征

IF 2.3 4区 工程技术 Q3 ENGINEERING, MANUFACTURING 3D Printing and Additive Manufacturing Pub Date : 2024-04-01 Epub Date: 2024-04-16 DOI:10.1089/3dp.2022.0118
Kerstin Dittmann, Steffen Czink, Stefan Dietrich, Anna Trauth, Kay André Weidenmann
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引用次数: 0

摘要

由于其非晶态结构,金属玻璃具有高强度、硬度和弹性应变极限等显著特性。相反,它们也表现出较高的脆性断裂敏感性,因此不太适合用作整体结构组件。因此,它们最好用作与韧性基体材料相结合的混合材料中的增强相。具有互穿结构的金属基复合材料尤其适用。这就要求金属玻璃具有开孔结构。在本研究中,采用激光粉末床熔融技术,用金属玻璃粉(Ni60Nb20Ta20)制造了一种开孔晶格结构。为了在保持金属玻璃无定形结构的同时制造出机械稳定的晶格结构,我们采用了各种扫描策略进行了参数研究。因此,进行了 X 射线衍射测量以验证参数研究。采用单扫描线和每层旋转 90° 的扫描策略,成功地实现了稳定的晶格结构,并在很大程度上保持了非晶结构。然而,在重新加热过程中,各印刷层之间形成的热影响区出现了 7% 的纳米结晶。在压缩试验中,0°方向的压缩模量达到 18 GPa,最大强度达到 90 MPa。在 90° 方向上,无法确定压缩模量,但压缩强度达到 15 兆帕。在进行纳米压痕测试时,打印的块状金属玻璃合金的杨氏模量为 195.1 GPa,维氏硬度为 HVIT = 956.1。通过差示扫描量热法对由此产生的晶格结构的热行为进行了进一步表征。
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Laser-Based Additive Manufacturing and Characterization of an Open-Porous Ni-Based Metallic Glass Lattice Structure (Ni60Nb20Ta20).

Due to their amorphous structure, metallic glasses exhibit remarkable properties such as high strength, hardness, and elastic strain limit. Conversely, they also exhibit high susceptibility to brittle fracture, making them less qualified for the use as monolithic structural components. Therefore, they may be preferably used as the reinforcing phase in hybrid materials combined with ductile matrix materials. Especially metal matrix composites with interpenetrating structures are suitable. This requires an open-porous structure of the metallic glass. In the study at hand, an open-porous lattice structure was manufactured from metallic glass powder (Ni60Nb20Ta20) by laser powder bed fusion. A parameter study was carried out with various scanning strategies to manufacture a mechanically stable lattice structure while maintaining the amorphous structure of the metallic glass. Thus, X-ray diffraction measurements were conducted to validate the parameter study. A stable lattice structure with a largely amorphous structure was successfully achieved with a scanning strategy of single scanned lines and a rotation of 90° for each layer. However, nanocrystallization of 7% occurred in the heat-affected zones formed between the individual printed layers during reheating. Conducting compression tests, a compressive modulus of 18 GPa and a maximum strength of 90 MPa in 0°-direction were achieved. In 90°-direction, no compressive modulus could be determined but compressive strength resulted in 15 MPa. Performing nanoindentation with a Young's modulus of 195.1 GPa and Vickers hardness of HVIT = 956.1 was achieved for the printed bulk metallic glass alloy. The resulting lattice structure was further characterized by differential scanning calorimetry for thermal behavior.

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来源期刊
3D Printing and Additive Manufacturing
3D Printing and Additive Manufacturing Materials Science-Materials Science (miscellaneous)
CiteScore
6.00
自引率
6.50%
发文量
126
期刊介绍: 3D Printing and Additive Manufacturing is a peer-reviewed journal that provides a forum for world-class research in additive manufacturing and related technologies. The Journal explores emerging challenges and opportunities ranging from new developments of processes and materials, to new simulation and design tools, and informative applications and case studies. Novel applications in new areas, such as medicine, education, bio-printing, food printing, art and architecture, are also encouraged. The Journal addresses the important questions surrounding this powerful and growing field, including issues in policy and law, intellectual property, data standards, safety and liability, environmental impact, social, economic, and humanitarian implications, and emerging business models at the industrial and consumer scales.
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