羟基磷灰石纳米棒对粉末冶金法制备Fe-14Mn-6Si合金烧结性能、硬度和生物活性的影响

M. Zawrah, Ibrahim Hassab Allahb, Ayman Abdellah Awad, Moataz H. Ata
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摘要

近年来,生产可生物降解的金属/陶瓷复合材料引起了工业界的极大兴趣。用铸造工具制备的铸造FeMn-Si合金生物降解率低;因此,寻找一种像粉末冶金(PM)这样的方法来制备具有更高生物可降解性的多孔体是很重要的。此外,羟基磷灰石(HA)纳米棒的加入提高了该合金的生物活性,形成了性能更好的复合材料。本研究采用PM法制备Fe-14Mn-6Si/HA复合材料,分别在1100、1150、1200C下进行烧结。研究了透明质酸纳米棒含量对复合材料物理性能、微观结构和显微硬度及生物活性的影响。结果表明:当烧结温度达到1150C时,体积密度随烧结温度的升高而增大;然后在1200℃时下降。堆积密度随HA含量的增加而增加。烧结后复合材料的硬度随烧结温度和HA用量的增加而增加。当HA含量为8%,烧结温度为1150℃和1200C时,试样的最大硬度值分别为1293和1792 MPa。制备的复合材料的生物活性随着HA用量的增加而增加。含8 wt.% HA的复合物生物活性最高。©2021由Sohag大学工程学院出版。DOI: 10.21608 / sej.2021.72585.1000
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Effect of hydroxyapatite nano rods on sinterability, hardness and bioactivity of Fe-14Mn-6Si alloy prepared by powder metallurgy
Recently, there is a great of industrial interest on the production of biodegradable metal/ceramic composites. The casted FeMn-Si alloys prepared by casting tools have low biodegradable rate; so it is important to seek a method as powder metallurgy (PM) to prepare porous bodies with increased biodegradability. Moreover, the addition of hydroxyapatite (HA) nano rods to that alloy increases its bioactivity and forms composite with improved properties. In the present study, Fe-14Mn-6Si/HA composites were prepared by PM and sintered at different temperatures, i.e. 1100, 1150 and 1200C. Also, the effect of HA nano-rods content on the composite properties (physical properties, microstructure and micro hardness) and bioactivity were studied. The results revealed that bulk density increased with increasing sintering temperature up to 1150C; then decreased at 1200C. Also, the bulk density increased with increasing the HA content. Moreover, the hardness of the sintered composites increased with increasing sintering temperature and HA amount. The maximum hardness values were 1293 & 1792 MPa for the specimens which contain 8 % HA and sintered at 1150 and 1200C, respectively. The bioactivity of the prepared composites increased with increasing HA amount. The highest bioactivity was for the composite that contains 8 wt.% HA. © 2021 Published by Published by Faculty of Engineering – Sohag University. DOI: 10.21608/sej.2021.72585.1000
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