{"title":"金属科学三维x射线衍射技术","authors":"Yubin Zhang, G. Fan","doi":"10.7502/J.ISSN.1674-3962.2017.03.04","DOIUrl":null,"url":null,"abstract":"Thethree-dimensionalX-raydifraction(3DXRD)isanew,advancedtechniqueformaterialscharacterization.This techniqueutilizeshigh-energysynchrotronX-raystocharacterizethe3Dcrystalographicstructureandstrain/stressstateofbulk materials.Asthemeasurementisnon-destructive,themicrostructuralevolutionasafunctionoftimecanbefolowed,ieit alows4D(x,y,zcharacterizations,t).ThehighbrilianceofsynchrotronX-raysensuresthatdifractionsignalsfrom volumesofmicrometerscalecanbequicklydetectedanddistinguishedfromthebackgroundnoise,ieitsspatialresolutioncan bemicrometerscaleandthemeasurementcanbeconductedwithinareasonabletimeframe(afewhours).The3DXRD microscopehasoriginalybeendevelopedincooperationbetweenformerRisNationalLaboratoryandtheEuropeanSynchrotron RadiationFacility.Curently,thistechniquehasbeenimplementedinseverallargesynchrotronfacilities,egtheAdvanced PhotonSource(APS)inUSAandtheSpring-8inJapan.Anotherfamilyof3DXRDtechniquethatutilizeswhitebeam synchrotronX-rayshasalsobeendevelopedinparalelincooperationbetweenOakRidgeNationalLaboratoryandAPS.This articlereviewsthe3DXRDtechnique.Thecontentincludestheideabehindthetechnique,theprincipleandspecification (spatial,angular,temporalresolutionsandsampleenvironmentetc)ofthetechnique.Severalapplicationsofthetechniquesin metalurgyaregiven,including:grain-scaledstressanalysisduringtensiledeformation,recrystalizationgrowthkinetics, recrystalizationnucleation,growthofindividualrecrystalizedgrain,graingrowthafterrecrystalization,andlocalresidualstrain/ stressanalysis.Therecentdevelopmentofthe3DXRDtechniqueanditspotentialuseformaterialsscienceinthefuturewilbe brieflydiscussedattheend.","PeriodicalId":53495,"journal":{"name":"中国材料进展","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2017-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Three-Dimensional X-Ray Diffraction Technique for Metals Science\",\"authors\":\"Yubin Zhang, G. Fan\",\"doi\":\"10.7502/J.ISSN.1674-3962.2017.03.04\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Thethree-dimensionalX-raydifraction(3DXRD)isanew,advancedtechniqueformaterialscharacterization.This techniqueutilizeshigh-energysynchrotronX-raystocharacterizethe3Dcrystalographicstructureandstrain/stressstateofbulk materials.Asthemeasurementisnon-destructive,themicrostructuralevolutionasafunctionoftimecanbefolowed,ieit alows4D(x,y,zcharacterizations,t).ThehighbrilianceofsynchrotronX-raysensuresthatdifractionsignalsfrom volumesofmicrometerscalecanbequicklydetectedanddistinguishedfromthebackgroundnoise,ieitsspatialresolutioncan bemicrometerscaleandthemeasurementcanbeconductedwithinareasonabletimeframe(afewhours).The3DXRD microscopehasoriginalybeendevelopedincooperationbetweenformerRisNationalLaboratoryandtheEuropeanSynchrotron RadiationFacility.Curently,thistechniquehasbeenimplementedinseverallargesynchrotronfacilities,egtheAdvanced PhotonSource(APS)inUSAandtheSpring-8inJapan.Anotherfamilyof3DXRDtechniquethatutilizeswhitebeam synchrotronX-rayshasalsobeendevelopedinparalelincooperationbetweenOakRidgeNationalLaboratoryandAPS.This articlereviewsthe3DXRDtechnique.Thecontentincludestheideabehindthetechnique,theprincipleandspecification (spatial,angular,temporalresolutionsandsampleenvironmentetc)ofthetechnique.Severalapplicationsofthetechniquesin metalurgyaregiven,including:grain-scaledstressanalysisduringtensiledeformation,recrystalizationgrowthkinetics, recrystalizationnucleation,growthofindividualrecrystalizedgrain,graingrowthafterrecrystalization,andlocalresidualstrain/ stressanalysis.Therecentdevelopmentofthe3DXRDtechniqueanditspotentialuseformaterialsscienceinthefuturewilbe brieflydiscussedattheend.\",\"PeriodicalId\":53495,\"journal\":{\"name\":\"中国材料进展\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2017-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"中国材料进展\",\"FirstCategoryId\":\"1087\",\"ListUrlMain\":\"https://doi.org/10.7502/J.ISSN.1674-3962.2017.03.04\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"Q3\",\"JCRName\":\"Energy\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"中国材料进展","FirstCategoryId":"1087","ListUrlMain":"https://doi.org/10.7502/J.ISSN.1674-3962.2017.03.04","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"Q3","JCRName":"Energy","Score":null,"Total":0}
引用次数: 0
Three-Dimensional X-Ray Diffraction Technique for Metals Science
Thethree-dimensionalX-raydifraction(3DXRD)isanew,advancedtechniqueformaterialscharacterization.This techniqueutilizeshigh-energysynchrotronX-raystocharacterizethe3Dcrystalographicstructureandstrain/stressstateofbulk materials.Asthemeasurementisnon-destructive,themicrostructuralevolutionasafunctionoftimecanbefolowed,ieit alows4D(x,y,zcharacterizations,t).ThehighbrilianceofsynchrotronX-raysensuresthatdifractionsignalsfrom volumesofmicrometerscalecanbequicklydetectedanddistinguishedfromthebackgroundnoise,ieitsspatialresolutioncan bemicrometerscaleandthemeasurementcanbeconductedwithinareasonabletimeframe(afewhours).The3DXRD microscopehasoriginalybeendevelopedincooperationbetweenformerRisNationalLaboratoryandtheEuropeanSynchrotron RadiationFacility.Curently,thistechniquehasbeenimplementedinseverallargesynchrotronfacilities,egtheAdvanced PhotonSource(APS)inUSAandtheSpring-8inJapan.Anotherfamilyof3DXRDtechniquethatutilizeswhitebeam synchrotronX-rayshasalsobeendevelopedinparalelincooperationbetweenOakRidgeNationalLaboratoryandAPS.This articlereviewsthe3DXRDtechnique.Thecontentincludestheideabehindthetechnique,theprincipleandspecification (spatial,angular,temporalresolutionsandsampleenvironmentetc)ofthetechnique.Severalapplicationsofthetechniquesin metalurgyaregiven,including:grain-scaledstressanalysisduringtensiledeformation,recrystalizationgrowthkinetics, recrystalizationnucleation,growthofindividualrecrystalizedgrain,graingrowthafterrecrystalization,andlocalresidualstrain/ stressanalysis.Therecentdevelopmentofthe3DXRDtechniqueanditspotentialuseformaterialsscienceinthefuturewilbe brieflydiscussedattheend.
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