溶剂热法合成银纳米颗粒的尺寸和形状控制

Nguyen Thi Ngoc Linh, Le The Tam, Ngo Thanh Dung, Le Thi Thanh Tam, Ha Minh Nguyet, Nguyen Dinh Vinh, Bui Minh Quy, Nguyen Thi Hong Hoa, Nguyen Hoa Du, Le Trong Lu, Nguyen Trung Thành
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引用次数: 0

摘要

在本研究中,在油酸钠(SOA)和十八醇(OCD-ol)存在的有机溶剂中,通过硝酸银的热分解制备了银纳米颗粒(NPs)。研究了不同溶剂和OCD-ol浓度对银纳米材料形貌和性能的影响。结构分析表明,银纳米材料具有良好的结晶度。样品的TEM图像表明,随着制备条件的改变,形成了不同尺寸和形状的银纳米材料。Ag纳米粒子的表面等离子体共振(SPR)特性受其尺寸和形状的影响。合成的银纳米粒子在生物医学、催化、电子等领域具有潜在的应用前景。
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The size-and shape-controlled synthesis of silver nanoparticles by solvothermal method
In this work, Ag nanoparticles (NPs) were fabricated by thermal decomposition of silver nitrate in organic solvents in the presence of sodium oleate (SOA) and 1-octadecanol (OCD-ol). The effects of different solvents and concentrations of OCD-ol on the morphology and properties of the Ag nanomaterials were investigated in detail. The structural analysis of the Ag nanomaterials showed good crystallinity. The TEM images of the samples showed that with the change in the fabrication conditions, different sizes and shapes of Ag nanomaterials were formed. The surface plasmon resonance (SPR) properties of the  Ag NPs were influenced by their size and shape. The as-synthesized Ag NPs have potential applications in biomedical, catalysis, or electronics.
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