合成和研究银纳米粒子的稳定性

R. Ridwan, Gusrizal Gusrizal, N. Nurlina, S. J. Santosa
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引用次数: 2

摘要

用水杨酸还原硝酸银,制备了水杨酸包封的纳米银。制备纳米银时,首先将硝酸银溶液与pH为11的水杨酸溶液按1:40的摩尔比混合。混合物在沸水浴中加热45分钟。银纳米粒子的形成由黄色的外观指示,并使用紫外可见分光光度计监测。所得银纳米粒子的最大峰出现在410 ~ 420 nm范围内,平均粒径为66±28 nm。16周的稳定性测试表明,水杨酸包覆的银纳米颗粒是稳定的。稳定性测试结果表明,水杨酸在银纳米颗粒的形成过程中同时具有还原和封盖作用。
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SINTESIS DAN STUDI STABILITAS NANOPARTIKEL PERAK TERTUDUNG ASAM SALISILAT
Silver nanoparticles capped with salicylic acid have been synthesized by reduction of silver nitrate with salicylic acid without additional capping agent. In the formation of silver nanoparticles, the solution of silver nitrate was first mixed with the pH 11 salicylic acid solutions at a mole ratio of 1:40. The mixture was heated for 45 minutes in a boiling water bath. The formation of silver nanoparticles was indicated by the appearance of yellow color and monitored using UV-Vis spectrophotometer. The maximum peak of resulted silver nanoparticles appeared in the range of 410-420 nm with the average size of particles was 66±28 nm. Stability test over a period of 16 weeks showed that silver nanoparticles capped with salicylic acid were stable. The results of stability test show that salicylic acid simultaneously act as reducing as well as capping agent in the formation of silver nanoparticles.
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