不同材料上粘接界面的磨损模式

A. Comba, A. Baldi, M. Bonito, E. Blanc, V. Notaro, M. Alovisi, D. Pasqualini, E. Berutti, N. Scotti
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摘要

目的:本体外研究的目的是研究上磨牙在循环咬合负荷下牙釉质-材料和牙本质-材料结合界面表面磨损的差异。方法:采用CAD-CAM技术和直接修复技术,采用不同的修复材料制备牙釉质-材料和牙本质-材料结合界面平面试件48个。在粘合和胶结过程后,用咀嚼机对不锈钢球进行平滑动接触测试(20N载荷,50,000次循环)。使用3D轮廓仪对牙釉质或牙本质基质和三种修复材料进行磨损分析和比较,并采用方差分析和事后比较程序进行分析。最后用光学显微镜检查磨损表面。结果:模拟咀嚼循环后的统计分析发现,“底物”因子(p<0.05)和“修复材料”因子(p<0.05)对咀嚼循环有显著影响。牙釉质比牙本质更耐磨性,也比所有的修复材料更耐磨性。在材料方面,微混杂复合膏体的磨损最为严重。CAD-CAM材料对牙本质和牙釉质的磨损率明显提高。在粘合界面层发现了一个有趣的磨损模式,从轮廓仪图像中获得的椭圆形强调了重复磨损模式,中心区域消耗更多,深度向周长移动。光学显微镜观察发现,釉质界面有裂纹的痕迹。结论:牙基体和修复材料对牙材料界面循环疲劳后的磨损行为均有显著影响。因此,最初的零假设被拒绝。
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Wear Patterns of Adhesive Interfaces over Different Materials
Purpose: The aim of this in vitro study was to investigate differences in surface wear of enamel-material and dentin-material bonded interfaces obtained from upper molars samples and subjected to cycling occlusal load. Methods: Forty-eight flat specimens of enamel-material and dentin-material bonded interfaces were prepared using different restorative materials with both CAD-CAM techniques and direct techniques. After the bonding and cementation procedures specimens were tested with a chewing machine with a stainless-steel ball on flat sliding contact (20N loads, 50.000 cycles). Wear analysis and comparison of the enamel or dentin substrates and the three restorative materials was performed using a 3D profilometer and analyzed with ANOVA test and post-hoc comparison procedures. Finally worn surfaces were examined with optical microscopy. Results: Statistical analysis after simulated chewing cycles identified a significant influence of the factor “substrate” (p<0.05) and of the factor “restorative material” (p<0.05). The enamel results in being more wear resistant than dentin, and also more resistant than all the restorative materials tested. Considering the materials, the most severe wear loss was observed with micro-hybrid composite paste. CAD-CAM materials showed a wear rate significantly better both in association with enamel and dentin. An interesting wear pattern was found at the bonded interface level and the oval shapes obtained from the profilometer images underlined a repetitive wear pattern with the central zone more consumed and decreasing depth moving towards the perimeter. Initials signs of cracks were showed in enamel interfaces at the optical microscopy analysis. Conclusions: Both the dental substrate and the restorative material significantly affect the wear behavior of a toothmaterial interface after cyclic fatigue. Thus, the initial null hypotheses were rejected.
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