氧化石墨烯对YBCO超导体关键参数的改善

B. Sahoo, S. Karmakar, D. Behera
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引用次数: 2

摘要

本文讨论了通过标准固相反应途径制备YBa2Cu3O7-δ高温超导体,并添加不同重量% (x = 0.0、0.1、0.3、0.5和0.7)的氧化石墨烯(GO)。通过x射线粉末衍射和场发射扫描电镜分别检测了复合材料的相纯度和表面形貌。自场输运测量和电场对电流密度测量证实了复合材料中超导性的存在。当氧化石墨烯添加量为0.7 wt. %时,临界温度的最大值为96.42 K。同样,在77K下,当氧化石墨烯添加量为0.7 wt. %时,观察到临界电流密度的最大值为412.92 A/cm2。这可能是由于氧化石墨烯位于晶界附近,增加了超导晶粒之间的弱连接,从而增强了样品的超导体积分数。本文讨论了通过标准固相反应途径制备YBa2Cu3O7-δ高温超导体,并添加不同重量% (x = 0.0、0.1、0.3、0.5和0.7)的氧化石墨烯(GO)。通过x射线粉末衍射和场发射扫描电镜分别检测了复合材料的相纯度和表面形貌。自场输运测量和电场对电流密度测量证实了复合材料中超导性的存在。当氧化石墨烯添加量为0.7 wt. %时,临界温度的最大值为96.42 K。同样,在77K下,当氧化石墨烯添加量为0.7 wt. %时,观察到临界电流密度的最大值为412.92 A/cm2。这可能是由于氧化石墨烯位于晶界附近,增加了超导晶粒之间的弱连接,从而增强了样品的超导体积分数。
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Improvement of critical parameters of YBCO superconductor by addition of graphene oxide
Here we discuss the preparation and characterization of YBa2Cu3O7-δ high temperature superconductor through standard solid state reaction route and added with different (x = 0.0, 0.1, 0.3, 0.5, & 0.7) wt. % of graphene oxide (GO). The phase purity and surface morphology of the composite samples were examined through the X-ray powder diffraction and Field emission scanning electron microscopy respectively. The self field transport measurement and electric field versus current density measurement confirms the occurrence of superconductivity in the composite materials. The maximum value of critical temperature is found to be 96.42 K for 0.7 wt. % GO added sample. Similarly, the maximum value of critical current density is observed to be 412.92 A/cm2 for 0.7 wt. % GO added sample at 77K. This may be attributed to enhancement in superconducting volume fraction of the sample, as GO resides near the grain boundary region to increase the weak link between the superconducting grains.Here we discuss the preparation and characterization of YBa2Cu3O7-δ high temperature superconductor through standard solid state reaction route and added with different (x = 0.0, 0.1, 0.3, 0.5, & 0.7) wt. % of graphene oxide (GO). The phase purity and surface morphology of the composite samples were examined through the X-ray powder diffraction and Field emission scanning electron microscopy respectively. The self field transport measurement and electric field versus current density measurement confirms the occurrence of superconductivity in the composite materials. The maximum value of critical temperature is found to be 96.42 K for 0.7 wt. % GO added sample. Similarly, the maximum value of critical current density is observed to be 412.92 A/cm2 for 0.7 wt. % GO added sample at 77K. This may be attributed to enhancement in superconducting volume fraction of the sample, as GO resides near the grain boundary region to increase the weak link between the superconducting grains.
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