溶胶-凝胶法合成的分散在二氧化硅中的银纳米粒子的杀菌作用

D. Mendiola, Ulises Arellano Sánchez, M. Palacios, Jin Wang, Li Fang Chen, F. Morales
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引用次数: 1

摘要

采用溶胶-凝胶法制备了含银量分别为2%、5%和10% w/w的SiO2纳米颗粒材料。将新鲜样品在500℃下用H2煅烧还原得到银。采用x射线衍射、N2物理吸附、紫外-可见光谱、电子透射显微镜和能谱仪对所得材料进行了研究。在大肠杆菌液相失活过程中观察抑菌活性,采用平板计数法鉴定活菌落形成单位(CFU)。结果表明,纳米银颗粒分散在SiO2中,随着纳米银颗粒含量和粒径的增加,其杀菌效率也随之提高。
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Bactericidal Action of Silver Nanoparticles Dispersed in Silica Synthesized through the Sol Gel Method
A series of Ag nanoparticle materials supported in SiO2 were synthesized by the sol-gel method, with contents of 2, 5 and 10% w/w. The fresh samples were calcinated and reduced with H2 at 500 °C in order to obtain Ag. The materials obtained were studied by X-ray diffraction, N2 physisorption, UV-vis spectroscopy, electronic transmission microscopy and EDS (energy dispersive spectrometer). The antibacterial activity was observed in the deactivation of E. coli in its liquid phase, using the plate count method to identify viable CFU (colony forming units). The results show that the materials containing Ag nanoparticles dispersed in SiO2 increase their bactericidal efficiency on the increase of the content and size of Ag nanoparticles.
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