六官能团环氧树脂的合成、表征、应用及与工业环氧树脂的比较

M. Raj, Jaykumar Maheta, L. Raj
{"title":"六官能团环氧树脂的合成、表征、应用及与工业环氧树脂的比较","authors":"M. Raj, Jaykumar Maheta, L. Raj","doi":"10.1177/09673911221076721","DOIUrl":null,"url":null,"abstract":"Current study compares the various analytical results of hexafunctional epoxy resins based on bisphenol-A with conventional epoxy resins. Reaction of bisphenol-A, formaldehyde, and epichlorohydrin produces hexafunctional epoxy resin. The curing properties of commercial epoxy resin and hexafunctional epoxy resin were determined using a variety of hardeners, including diethylenetriamine, triethylenetetramine, phenalkamine, polyamido amines, and polyamides. The epoxy equivalent weight (EEW), hydrolyzable chlorine content, volatile content, Brookfield viscosity, weight average molecular weight, elemental analysis (C, H, N, O analysis), and Fourier transform infrared spectroscopy were used to characterize the hexafunctional resin (FT-IR). Jute and glass reinforced composites were also prepared by using hexafunctional epoxy resins and commercial epoxy resins. Mechanical properties (tensile strength, flexural strength, Izod impact strength, and Rockwell hardness), thermal properties, and chemical resistance were determined for each composite. Hexafunctional epoxy resin-based composites exhibited superior mechanical characteristics, thermal resistance, and chemical resistance properties than commercial epoxy resin-based composites.","PeriodicalId":20417,"journal":{"name":"Polymers and Polymer Composites","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2022-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"Synthesis characterization and application of hexafunctional epoxy resin and comparison against commercial epoxy resin\",\"authors\":\"M. Raj, Jaykumar Maheta, L. Raj\",\"doi\":\"10.1177/09673911221076721\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Current study compares the various analytical results of hexafunctional epoxy resins based on bisphenol-A with conventional epoxy resins. Reaction of bisphenol-A, formaldehyde, and epichlorohydrin produces hexafunctional epoxy resin. The curing properties of commercial epoxy resin and hexafunctional epoxy resin were determined using a variety of hardeners, including diethylenetriamine, triethylenetetramine, phenalkamine, polyamido amines, and polyamides. The epoxy equivalent weight (EEW), hydrolyzable chlorine content, volatile content, Brookfield viscosity, weight average molecular weight, elemental analysis (C, H, N, O analysis), and Fourier transform infrared spectroscopy were used to characterize the hexafunctional resin (FT-IR). Jute and glass reinforced composites were also prepared by using hexafunctional epoxy resins and commercial epoxy resins. Mechanical properties (tensile strength, flexural strength, Izod impact strength, and Rockwell hardness), thermal properties, and chemical resistance were determined for each composite. Hexafunctional epoxy resin-based composites exhibited superior mechanical characteristics, thermal resistance, and chemical resistance properties than commercial epoxy resin-based composites.\",\"PeriodicalId\":20417,\"journal\":{\"name\":\"Polymers and Polymer Composites\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Polymers and Polymer Composites\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1177/09673911221076721\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Polymers and Polymer Composites","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1177/09673911221076721","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 3

摘要

本研究比较了双酚a基六官能环氧树脂与常规环氧树脂的各种分析结果。双酚a、甲醛和环氧氯丙烷反应生成六官能团环氧树脂。采用不同的硬化剂,包括二乙烯三胺、三乙烯四胺、苯烷胺、聚胺胺和聚酰胺,测定了工业环氧树脂和六功能环氧树脂的固化性能。采用环氧当量(EEW)、可水解氯含量、挥发分含量、布鲁克菲尔德粘度、重量平均分子量、元素分析(C、H、N、O分析)和傅里叶变换红外光谱(FT-IR)对六官能层树脂进行表征。用六官能环氧树脂和工业环氧树脂制备了黄麻和玻璃增强复合材料。测定了每种复合材料的机械性能(拉伸强度、弯曲强度、Izod冲击强度和洛氏硬度)、热性能和耐化学性。六官能团环氧树脂基复合材料具有比普通环氧树脂基复合材料更好的机械性能、耐热性和耐化学性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
查看原文
分享 分享
微信好友 朋友圈 QQ好友 复制链接
本刊更多论文
Synthesis characterization and application of hexafunctional epoxy resin and comparison against commercial epoxy resin
Current study compares the various analytical results of hexafunctional epoxy resins based on bisphenol-A with conventional epoxy resins. Reaction of bisphenol-A, formaldehyde, and epichlorohydrin produces hexafunctional epoxy resin. The curing properties of commercial epoxy resin and hexafunctional epoxy resin were determined using a variety of hardeners, including diethylenetriamine, triethylenetetramine, phenalkamine, polyamido amines, and polyamides. The epoxy equivalent weight (EEW), hydrolyzable chlorine content, volatile content, Brookfield viscosity, weight average molecular weight, elemental analysis (C, H, N, O analysis), and Fourier transform infrared spectroscopy were used to characterize the hexafunctional resin (FT-IR). Jute and glass reinforced composites were also prepared by using hexafunctional epoxy resins and commercial epoxy resins. Mechanical properties (tensile strength, flexural strength, Izod impact strength, and Rockwell hardness), thermal properties, and chemical resistance were determined for each composite. Hexafunctional epoxy resin-based composites exhibited superior mechanical characteristics, thermal resistance, and chemical resistance properties than commercial epoxy resin-based composites.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
期刊最新文献
Modelling and characterising FFF process of semi-crystalline polymers: Warpage formation and mechanism analysis Machine learning non-isothermal study of the blade coating process (NIS-BCP) using non-Newtonian nanofluid with magnetohydrodynamic (MHD) and slip effects Performance of polyurethane and polyurethane nanocomposites modified by graphene, carbon nanotubes, and fumed silica in dry and wet environments Effect of hybrid weaving patterns on mechanical performance of 3D woven structures Investigation of effects of bis(2-hydroxyethyl) terephthalate derived from glycolysis of polyethylene terephthalate on the properties of flexible polyurethane foam
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
已复制链接
已复制链接
快去分享给好友吧!
我知道了
×
扫码分享
扫码分享
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1