陶瓷法合成Ni0.7Zn0.3Fe2O4+0.4wt%V2O5的结构、红外和磁性能

M. S. Patil, A. Patil, D. P. Nandagawali, A. V. Raut, D. R. Shengule
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摘要

在本研究中,我们旨在通过陶瓷技术合成添加0.4wt%V2O5的Ni0.7Zn0.3Fe2O4,并通过各种表征技术测定其结构磁性和介电性能。用x射线衍射技术鉴定了添加V2O5后的相杂质。用红外光谱法对其进行了官能团分析和相形成的确定。XRD分析表明,所有样品均具有单相立方尖晶石结构。根据XRD数据计算了晶格常数(a)和x射线密度(dx)。采用脉冲场磁滞回线测量技术研究了Ni0.7Zn0.3Fe2O4+0.4wt%V2O5的磁性能。我们报道了Ni0.7Zn0.3Fe2O4+0.4wt%V2O5的饱和磁化强度(Ms)、剩磁磁化强度(Mr)和磁子数(nB)的增加是V2O5添加的原因。而磁性参数的改变则导致矫顽力(Hc)的急剧下降。研究了0.4wt%V2O5添加剂对Ni0.7Zn0.3Fe2O4铁氧体物理性能的影响。
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Structural, infrared and magnetic properties of Ni0.7Zn0.3Fe2O4+0.4wt%V2O5 synthesized using ceramic method
In this investigation, we aimed to synthesize Ni0.7Zn0.3Fe2O4 added with 0.4wt%V2O5 by ceramic technique and the structural magnetic and dielectric properties are determined by various characterization techniques. The phase impurity over the addition of V2O5 was identified by X-ray diffraction technique. The functional group analysis by locating the absorption bands and confirmation of formation of phase was examined by infrared spectroscopy. XRD pattern reveals that all the samples have single-phase cubic spinel structure. The lattice constant (a) and x-ray density (dx) were calculated from the XRD data. Magnetic properties of Ni0.7Zn0.3Fe2O4+0.4wt%V2O5 were carried out by pulse field hysteresis loop measurement technique. We report an increase in the Saturation magnetization (Ms), Remanence magnetization (Mr) and magneton number (nB) of Ni0.7Zn0.3Fe2O4+0.4wt%V2O5 as a cause of V2O5 addition. Whereas, the value of coercivity (Hc) was drastically decreased suggesting the changed magnetic parameters. This investigation focused on the characteristic effect of additive 0.4wt%V2O5 on physical properties of Ni0.7Zn0.3Fe2O4 ferrite.
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