用非热等离子体系统在玻璃纤维上沉积石墨烯

Paulo V. R. Gomes, R. N. Bonifácio, Barbara P. G. Silva, J. C. Ferreira, R. D. de Souza, L. Otubo, D. Lazar, A. O. Neto
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引用次数: 0

摘要

本研究报告了一种自下而上的方法,将环己烷转化为石墨烯纳米片,然后使用非热发生器将其沉积在玻璃纤维上。通过透射电镜对复合材料进行了表征,结果表明,复合材料形成了部分无序的叠层石墨烯,层间的d间距为0.358 nm。x射线衍射证实了TEM图像的观察结果。SEM图像显示,碳质材料在玻璃纤维上聚集,由于合成方法的原因,玻璃纤维发生了一定的分层。拉曼光谱分析表明,制备的石墨烯在结构上以缺陷为主。此外,原子力显微镜(AFM)分析揭示了具有不同孔隙度的石墨烯层的形成。
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Graphene Deposited on Glass Fiber Using a Non-Thermal Plasma System
This study reports a bottom-up approach for the conversion of cyclohexane into graphene nanoflakes, which were then deposited onto fiberglass using a non-thermal generator. The composite was characterized using transmission electron microscopy, which revealed the formation of stacked few-layer graphene with a partially disordered structure and a d-spacing of 0.358 nm between the layers. X-ray diffraction confirmed the observations from the TEM images. SEM images showed the agglomeration of carbonaceous material onto the fiberglass, which experienced some delamination due to the synthesis method. Raman spectroscopy indicated that the obtained graphene exhibited a predominance of defects in its structure. Additionally, atomic force microscopy (AFM) analyses revealed the formation of graphene layers with varying levels of porosity.
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