E. T. Aslanova, E.T. Mamedov, M. Rashidova, A. Garayeva, V.O. Atakishiyeva
{"title":"以糖精-6-羧酸2-羟丙基-1,3-双羧甲基酯磺酰亚胺为原料合成新型耐热性多羟基酯","authors":"E. T. Aslanova, E.T. Mamedov, M. Rashidova, A. Garayeva, V.O. Atakishiyeva","doi":"10.32737/2221-8688-2023-2-140-145","DOIUrl":null,"url":null,"abstract":"By polycondensation of 2-hydroxypropyl-1,3-bis-carboxymethylesterosulfoimide of saccharin-6- carboxylic acid with ethylene glycol, a thermostable polyhydroxyester was obtained. The structure of the synthesized compound was confirmed by data of the infrared spectroscopy and the thermal stability studied by a method of differential-thermal analysis on a derivatograph of “Paulik—Paulik Erdei” system. The derivatographic investigations showed that the synthesized polyhydroxyester had high thermal stability and physical-mechanical properties.","PeriodicalId":10015,"journal":{"name":"Chemical Problems","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2023-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"SYNTHESIS OF NEW THERMOSTABLE POLYHYDROXYESTER ON THE BASIS OF 2- HYDROXYPROPYL-1,3-BIS-CARBOXYMETHYLESTEROSULFOIMIDE OF SACCHARIN-6-CARBOXYLIC ACID\",\"authors\":\"E. T. Aslanova, E.T. Mamedov, M. Rashidova, A. Garayeva, V.O. Atakishiyeva\",\"doi\":\"10.32737/2221-8688-2023-2-140-145\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"By polycondensation of 2-hydroxypropyl-1,3-bis-carboxymethylesterosulfoimide of saccharin-6- carboxylic acid with ethylene glycol, a thermostable polyhydroxyester was obtained. The structure of the synthesized compound was confirmed by data of the infrared spectroscopy and the thermal stability studied by a method of differential-thermal analysis on a derivatograph of “Paulik—Paulik Erdei” system. The derivatographic investigations showed that the synthesized polyhydroxyester had high thermal stability and physical-mechanical properties.\",\"PeriodicalId\":10015,\"journal\":{\"name\":\"Chemical Problems\",\"volume\":null,\"pages\":null},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-01-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Chemical Problems\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.32737/2221-8688-2023-2-140-145\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Chemical Problems","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.32737/2221-8688-2023-2-140-145","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
SYNTHESIS OF NEW THERMOSTABLE POLYHYDROXYESTER ON THE BASIS OF 2- HYDROXYPROPYL-1,3-BIS-CARBOXYMETHYLESTEROSULFOIMIDE OF SACCHARIN-6-CARBOXYLIC ACID
By polycondensation of 2-hydroxypropyl-1,3-bis-carboxymethylesterosulfoimide of saccharin-6- carboxylic acid with ethylene glycol, a thermostable polyhydroxyester was obtained. The structure of the synthesized compound was confirmed by data of the infrared spectroscopy and the thermal stability studied by a method of differential-thermal analysis on a derivatograph of “Paulik—Paulik Erdei” system. The derivatographic investigations showed that the synthesized polyhydroxyester had high thermal stability and physical-mechanical properties.
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