硼水钠浓度对微乳法合成纳米硅的影响

W. Liong, S. Sreekantan, S. D. Hutagalung
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引用次数: 5

摘要

报道了硼水钠(NaBH4)还原剂浓度对微乳法制备纳米硅性能的影响。以四氯化硅(SiCl4)为硅源,氢氧化钠(NaOH)为稳定剂,聚乙二醇(PEG)为表面活性剂,保持其浓度不变。合成了4个nabh4浓度为0.05 ~ 0.20 M的样品。结果表明,最低浓度的NaBH4有利于硅纳米颗粒的形成。
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Effect of Concentration of Sodium Borohydrate on the Synthesis of Silicon Nanoparticles via Microemulsion Route
The effect of concentration of reduction agent of sodium borohydrate (NaBH4) on the properties of silicon nanoparticles synthesized via microemulsion route is reported. In this work, the concentration of the silicon tetrachloride (SiCl4) that served as silicon source with sodium hydroxide (NaOH) and polyethylene glycol (PEG) as stabilizer and surfactant, respectively, are keep fixed. Four samples with varied concentration of NaBH4 from 0.05 M to 0.20 M were synthesized. It was found that the lowest concentration of NaBH4 gave better formation of silicon nanoparticles.
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