纳米板Bi2WO6作为氢探测纳米传感器的电导传感特性

R. Radha, R. A. Rakkesh, S. Balakumar
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引用次数: 2

摘要

本文采用易共沉淀法合成了Bi2WO6纳米薄片,然后利用超声波对沉淀物进行物理处理。x射线衍射(XRD)结果证实了Bi2WO6的正交结构,而场发射扫描电镜(FESEM)图像显示了纳米血小板的形态。用x射线光电子能谱(XPS)进行化学分析。探讨了超声-共沉淀法制备Bi2WO6纳米薄片的机理。首次以氢气为靶气体,对合成的Bi2WO6纳米片的气敏性能进行了分析。有趣的是,与现有的报告相比,工作温度的显著降低已经证明了这一机制。本文采用易共沉淀法合成了Bi2WO6纳米薄片,然后利用超声波对沉淀物进行物理处理。x射线衍射(XRD)结果证实了Bi2WO6的正交结构,而场发射扫描电镜(FESEM)图像显示了纳米血小板的形态。用x射线光电子能谱(XPS)进行化学分析。探讨了超声-共沉淀法制备Bi2WO6纳米薄片的机理。首次以氢气为靶气体,对合成的Bi2WO6纳米片的气敏性能进行了分析。有趣的是,与现有的报告相比,工作温度的显著降低已经证明了这一机制。
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Conductometric sensing characteristics of nanoplatelet Bi2WO6 as nanosensor for hydrogen detection
In this work, nanoplatelets of Bi2WO6 were synthesized by facile co-precipitation method followed by physical processing of the precipitate using ultrasonic waves. The X-Ray diffraction (XRD) results confirmed the orthorhombic structure of Bi2WO6, whereas the field emission scanning electron microscopy (FESEM) images revealed nanoplatelet morphology. Chemical analysis was done using X-ray photoelectron spectroscopy (XPS). Thus formation mechanism Bi2WO6 nanoplatelets (NPs) by the method of co-precipitation coupled with ultrasonic waves has been discussed. Gas sensing property of as synthesized Bi2WO6 nanoplatelets was analysed using hydrogen as target gas, a first of its kind. Interestingly a significant decrease in operating temperature was noticed when compared to the available reports for which the mechanism has been demonstrated.In this work, nanoplatelets of Bi2WO6 were synthesized by facile co-precipitation method followed by physical processing of the precipitate using ultrasonic waves. The X-Ray diffraction (XRD) results confirmed the orthorhombic structure of Bi2WO6, whereas the field emission scanning electron microscopy (FESEM) images revealed nanoplatelet morphology. Chemical analysis was done using X-ray photoelectron spectroscopy (XPS). Thus formation mechanism Bi2WO6 nanoplatelets (NPs) by the method of co-precipitation coupled with ultrasonic waves has been discussed. Gas sensing property of as synthesized Bi2WO6 nanoplatelets was analysed using hydrogen as target gas, a first of its kind. Interestingly a significant decrease in operating temperature was noticed when compared to the available reports for which the mechanism has been demonstrated.
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