热分析技术及样品杯的现状与发展

Chen Li, Dayong Li, D. Shi, B. Lu
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引用次数: 0

摘要

本文简要介绍了热分析的基本原理和热分析装置的结构。总结了不同材料和温度传感器制成的热分析样品杯的结构和性能,指出了它们的优缺点。详细介绍了树脂砂热电偶样品杯和石墨热电偶样品杯。热分析装置主要由样品杯和数据采集处理系统组成,热电偶预嵌在样品杯中监测温度。树脂砂杯在一次性使用的同时被广泛使用。虽然石墨样品杯和铜样品杯可以重复使用,但它们只能用于铝合金的热分析。
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Current situation and development of thermal analysis technology and sample cup
In this paper, the basic principles of thermal analysis and the structure of thermal analysis device are briefly reviewed. The structure and properties of thermal analysis sample cup made of different materials and temperature sensor are summarized, and their advantages and disadvantages are indicated. Also, the thermocouple sample cup made of resin sand and thermocouple sample cup made of graphite are described in detail. Thermal analysis device is mainly composed of the sample cup and data acquisition and processing system, and the thermocouples are pre-embedded in the cup to monitor the temperature. The resin sand cup is widely used while it is disposable. Although the graphite sample cup and Cu sample cup can be reused, they can only be used in the thermal analysis of aluminum alloys.
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