基于C12880MA和C11708MA微型光谱仪的漫反射分光光度计

IF 0.2 Q4 INSTRUMENTS & INSTRUMENTATION Devices and Methods of Measurements Pub Date : 2022-07-06 DOI:10.21122/2220-9506-2022-13-2-93-104
V. Firago, N. Levkovich, K. Shuliko
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引用次数: 1

摘要

具有空间分辨率的漫反射光谱是无损控制包括食品在内的许多散射细分散材料特性的一个有前途的方向。它可以找到广泛的实际应用,只有在存在的紧凑,易于使用和廉价的分光光度计设备。本文的目的是研究在滨松微型光谱仪的基础上,与现代计算设备一起工作的便携式分光光度计的可能性。综述了C12880MA和C11708MA微型光谱仪与便携式计算设备的连接原理图。展示了在STM32F103C8T6芯片上使用小型微处理器板ARM STM32F103C8T6 (Blue pill)的可行性。它在连接方案中的使用简化了通过USB接口与控制计算机的数据交换和控制微型光谱仪所需的所有信号的形成。制作了基于C12880MA和C11708MA微型光谱仪和STM32微处理器的两种分光光度计实验样品,并对其特性进行了研究。介绍了这些分光光度计的校准程序和软件的特点。所描述的特征保证了软件修改对所要解决的分光光度问题的效率。在C12880MA光谱范围的短波部分发现了配准光谱的畸变。它们是由于凹衍射光栅将被它散射的一部分辐射聚焦到零阶而产生的。基于Hamamatsu微型光谱仪研制的便携式分光光度计的批准,表明了其在便携式分光光度计设备和散射材料光学特性光谱控制装置中的应用可能性。所描述的校准技术允许您确定光谱的范围,其中记录的光谱失真最小。提出的解决方案显著降低了空间分辨率漫反射光谱器件的成本,并扩大了其在科学和工业各个分支中使用的可能性。
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Diffuse Reflectance Spectrophotometers Based on C12880MA and C11708MA Mini-Spectrometers Hamamatsu
Diffuse reflection spectroscopy with spatial resolution is a promising direction of non-destructive control of the properties of a number of scattering fine-dispersed materials, including food products. It can find wide practical application only in the presence of compact, easy-to-use and inexpensive spectrophotometric equipment. The aim of the article is to investigate the possibility of creating portable spectrophotometers based on Hamamatsu mini-spectrometers, which work together with modern computing facilities.The schematics for connecting the C12880MA and C11708MA mini-spectrometers to portable computing devices are reviewed. Shows the feasibility of using a small-sized microprocessor board ARM STM32F103C8T6 (Blue pill) on the chip STM32F103C8T6. Its use in the connection scheme has simplified data exchange with the control computer via USB interface and the formation of all the signals that are needed to control the mini-spectrometer.Two experimental samples of spectrophotometers based on C12880MA and C11708MA mini-spectrometers and STM32 microprocessors were created and their characteristics were studied. The calibration procedure and features of the software for these spectrophotometers are presented. The described features ensure the efficiency of software modification for the spectrophotometric problem to be solved. The presence of distortions of the registered spectra in the short-wave part of the spectral range of C12880MA was revealed. They arise due to focusing by the concave diffraction grating of a part of the radiation scattered by it into zero order.Approbation of developed portable spectrophotometers based on Hamamatsu mini-spectrometers indicates the possibility of their use in portable spectrophotometric equipment and devices for spectral control of optical properties of scattering materials. The described calibration technique allows you to determine the range of the spectrum, in which the distortions of the recorded spectra are minimal. The proposed solutions significantly reduce the cost of diffuse reflectance spectroscopy devices with spatial resolution and expand the possibilities of their use in various branches of science and industry.
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来源期刊
Devices and Methods of Measurements
Devices and Methods of Measurements INSTRUMENTS & INSTRUMENTATION-
自引率
25.00%
发文量
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审稿时长
8 weeks
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