空束棕榈油中钾含量的测定采用火焰光度法

S. Alva
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摘要

研究了用火焰光度法测定空束棕榈油中钾的含量。样本随机采集于苏门答腊北部海拔< 25 ~ 400 m的5个不同海拔区域。第一次取样在丹戎巴莱< 25米的拿督班达区,在基萨兰50至100米的莫兰蒂区,在Simalungun 150至200米的Bosar Maligas区,在Pematang Siantar 250至300米的Simarimbun区,以及在Sidamanik 350至400米的Sari Matondang区。样品用浓硝酸和30%双氧水消化,加入浓硝酸加热。采用标定方法,用火焰光度计在特定波长767.5 nm处测定钾含量。结果表明:样品中钾含量为11.83%;17.56%;21.89%;丹戎巴莱、基沙兰、西马伦贡、培马当辛达和西达马尼分别为24.68%和25.14%。得到的数据表明,海水面积越高,温度越低,因此棕榈油空束中的钾含量增加。
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Determination of Potassium in Empty Bunches Palm Oil (Elaeis guineensis Jacq.) Using Flame Photometry Method
Research on the determination of potassium in empty bunches palm oil have been done with the flame photometry method. The samples were taken randomly from five areas in Northen Sumatera with various heights in the range of < 25- 400 m above sea level. The first sampling was of Datuk Bandar district at Tanjung Balai < 25 m, Meranti district at Kisaran 50 to 100 m, Bosar Maligas district at Simalungun 150-200 m, Simarimbun district at Pematang Siantar 250 to 300 m, and the last Sari Matondang district at Sidamanik 350-400 m. The sample was digested using concentrated nitric aid and 30% hydrogen peroxide then heated with the addition of nitric acid concentrated. Potassium content was measured with a flame photometer at specific 767.5 nm by using calibration methods. The result obtained that potassium contents in the samples were 11.83%; 17.56%; 21.89%; 24.68%, and 25.14% for Tanjung Balai, Kisaran, Simalungun, Pematang Siantar, and Sidamanik respectively. The data obtained showed the higher area of the sea, the lower the temperature so the content of potassium increased in the palm oil empty bunches.
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