{"title":"大环二烯的合成及其与马来酸酐的反应","authors":"R. Ingraham, D. M. Macdonald, K. Wiesner","doi":"10.1139/CJR50B-055","DOIUrl":null,"url":null,"abstract":"Cyclotetradecanol–on–2 was dehydrated in the gas phase to cyclotetradecen–one–3. The latter was reduced with lithium aluminum hydride to cyclotetradecen–ol–3, which was converted by dehydration to cyclotetradecadiene. This compound gave with maleic anhydride 3-6-decamethylene tetrahydrophthallic anhydride. The same series of reactions was performed in the cyclooctadecane series.","PeriodicalId":9392,"journal":{"name":"Canadian journal of research","volume":"68 1","pages":"453-459"},"PeriodicalIF":0.0000,"publicationDate":"1950-08-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"3","resultStr":"{\"title\":\"SYNTHESIS OF LARGE RING DIENES AND THEIR REACTION WITH MALEIC ANHYDRIDE\",\"authors\":\"R. Ingraham, D. M. Macdonald, K. Wiesner\",\"doi\":\"10.1139/CJR50B-055\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Cyclotetradecanol–on–2 was dehydrated in the gas phase to cyclotetradecen–one–3. The latter was reduced with lithium aluminum hydride to cyclotetradecen–ol–3, which was converted by dehydration to cyclotetradecadiene. This compound gave with maleic anhydride 3-6-decamethylene tetrahydrophthallic anhydride. The same series of reactions was performed in the cyclooctadecane series.\",\"PeriodicalId\":9392,\"journal\":{\"name\":\"Canadian journal of research\",\"volume\":\"68 1\",\"pages\":\"453-459\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"1950-08-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"3\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Canadian journal of research\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1139/CJR50B-055\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Canadian journal of research","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1139/CJR50B-055","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
SYNTHESIS OF LARGE RING DIENES AND THEIR REACTION WITH MALEIC ANHYDRIDE
Cyclotetradecanol–on–2 was dehydrated in the gas phase to cyclotetradecen–one–3. The latter was reduced with lithium aluminum hydride to cyclotetradecen–ol–3, which was converted by dehydration to cyclotetradecadiene. This compound gave with maleic anhydride 3-6-decamethylene tetrahydrophthallic anhydride. The same series of reactions was performed in the cyclooctadecane series.
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