提高井筒稳定性的粘土-流体相互作用实验研究

M. Al-Arfaj, Amanullah
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引用次数: 1

摘要

由于水与粘土矿物发生反应,使用水基钻井液钻井页岩地层会导致井筒稳定性问题。当粘土与水接触时,粘土开始反应、膨胀和/或分散,导致页岩解体和脱落。因此,井眼可能会变得更紧,井眼中可能会出现更高的固体载荷,因此,卡钻的可能性会增加,钻井液的井眼清洁效率会显著降低。本文描述了在四个页岩样品上进行的实验工作,以评估粘土-流体相互作用和页岩稳定性。在进行x射线衍射矿物学分析后,采用去离子水、5%氯化钾卤水和5%多胺溶液进行分散性和溶胀性页岩抑制试验。这项工作已扩展到不同的纯粘土样品:钠蒙脱土、伊利石和伊利石蒙脱石混合层。阳离子交换容量结果表明,蒙脱土和伊利蒙石混合层在自然条件下更愿意交换阳离子,吸附水分,具有较高的反应活性。同样,蒙脱石和伊利-蒙脱石浓度越高的页岩样品CEC值越高。分散试验结果表明,以高岭石为主的页岩回收率为30.8%,低高岭石含量的页岩回收率为98.65%。对于高高岭石样品,采用氯化钾溶液回收率由30.8%提高到59%,采用多胺溶液回收率达到85.5%。在膨胀仪中测试样品时,结果显示蒙脱石含量高的样品膨胀率较高,其次是伊利石,而粘土含量较低,小于15%,两种样品没有潜在的膨胀。
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Experimental Investigation on Clay-Fluid Interactions for Enhanced Wellbore Stability
The use of water-based drilling fluids to drill shale formations causes wellbore stability problems as a result of the reaction of water with clay minerals. When it comes in contact with water, clay starts to react, swell and/or disperse leading to shale disintegration and sloughing. Consequently, tight hole might develop and/or higher solids loading in the wellbore might be experienced and, hence, the chance to get stuck pipe increases and the hole cleaning efficiency of drilling fluid decreases significantly. This paper describes the experimental work conducted on four shale samples to assess clay-fluid interactions and shale stabilization. After conducting mineralogical analysis using X-ray diffraction, shale inhibition tests including dispersion and swelling tests were carried out using de-ionized water, 5% potassium chloride brine and 5% Polyamines solution. The work has been extended to cover different pure clay samples: sodium montmorillonite, illite and illite smectite mixed layer. Cation exchange capacity results showed high reactivity in sodium montmorillonite and illite-smectite mixed layer as they are more willing to exchange cations and adsorb water at natural conditions. Similarly, shale samples with higher concentration of smectite and illite-smectite showed higher CEC values. Dispersion results showed that shale recovery percentages varied from 30.8% for shale sample dominated by kaolinite to 98.65% for those with low kaolinite content. For the high kaolinite sample, the recovery percentage jumped from 30.8% to 59% with potassium chloride and eventually to 85.5% when the polyamine solution was used. When the samples were tested in the swell meter, results showed higher swelling percentage values for those samples with higher smectite content followed by illite while two samples showed no potential swelling as they have low clay content of less than 15%.
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