玫瑰挥发油成分:蒸馏方法对品质的影响

K. Hosni, Amel Kerkenni, Wafa Medfei, N. Brahim, H. Sebei
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引用次数: 27

摘要

采用加氢蒸馏法(HD)和传统干馏法(DD)分离纯化了牛蒡花挥发油,并采用HRGC-FID和GC-MS对其进行了分析。与HD相比,DD在50°C下可分离出含氧化合物含量最高(83%)的高质量油。主要成分为2-苯乙醇和丁香酚。2-苯乙醇是玫瑰精油中非常理想的成分,在DD提取物中所占的比例(58.4%)明显高于HD提取物(13.6%)。随着DD过程中温度的升高(100℃),油品质量下降。2-苯乙醇含量变化最显著(4.5%)。此外,还观察到烷烃和呋喃衍生物的产量增加。因此,中等温度(50℃)的DD处理更适合改善牛蒡的挥发油品质,从而使其发挥更大的价值。
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Volatile Oil Constituents of Rosa canina L.: Quality As Affected by the Distillation Method
The volatile oils of R. canina flowers were isolated by hydrodistillation (HD) and traditional dry distillation (DD) and analyzed by HRGC-FID and GC-MS. Compared to HD, DD at 50°C leads to the isolation of high quality oil which contains the highest content of oxygenated compounds (83%). The main components are the 2-phenethyl alcohol and eugenol. The percentage of the 2-phenethyl alcohol, a highly desirable component in rose oil, was significantly higher (58.4%) in DD extract when compared to that of HD one (13.6%). As temperature increased (100°C) during DD, the oil quality decreased. The most significant changes were observed in 2-phenethyl alcohol percentage (4.5%). Moreover, an increase of alkanes/alkenes and the production of furan derivatives were observed. So, DD at moderate temperature (50°C) seemed more suitable to improve the volatile oil quality and hence, to make more value of R. canina.
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