基于小型拉曼光谱系统的爆炸物对峙拉曼探测

N. Hadi, M. R. Mohammad, Haider G. Abdulzahraa
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引用次数: 5

摘要

在此工作中,设计、组装并测试了一个对峙拉曼光谱SRS系统,用于在黑暗实验室中4米目标望远镜距离上检测爆炸物(硝酸铵、三硝基甲苯和硝酸尿素)。SRS系统采用倍频Nd:YAGlaser,激发波长为532 nm,激光功率为250 mW,积分时间为2秒。采用光纤电缆将卡塞格伦望远镜与文塔纳拉曼光谱仪耦合,利用陷波滤波器抑制瑞利散射光。拉曼散射光由望远镜采集,经光纤传输到光谱仪,最后进入电荷耦合器件CCD探测器。为了测试SRS系统,它已被用于检测有毒工业化合物TIC如丙酮,甲苯和四氯化碳的拉曼光谱。使用台式Bruker SENTERRA拉曼仪器将SRS结果与传统拉曼显微镜结果进行比较。
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Standoff Raman Detection of Explosive Materials Using a Small Raman Spectroscopy System
In this work a standoff Raman spectroscopy SRS system has been designed, assembled andtested for detecting explosives (Ammonium nitrate, Trinitrotoluene and Urea nitrate) in darklaboratory at 4 m target-telescope distance. The SRS system employs frequency doubled Nd:YAGlaser at 532 nm excitation with laser power of 250 mW and integration time of 2 second. The Cassegrain telescope was coupled to the Ventana Raman spectrometer using a fiber optics cable, and Notch filter is used to reject Rayleigh scattering light. The Raman scattered light is collected by a telescope and then transferred via fiber optic to spectrometer and finally directed into charge coupled device CCD detector. In order to test SRS system, it has been used to detect the Raman spectra of Toxic Industrial Compounds TIC such as acetone, toluene, and carbon tetrachloride. The SRS results were compared with conventional Raman microscopy results using a bench top Bruker SENTERRA Raman instrument.
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