液氮中Au-Co合金高压扭转过程中剪切应力的压力依赖性

T. Tolmachev, V. Pilyugin, A. M. Patselov, N. Nikolayeva, A. Vlasova
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引用次数: 0

摘要

首次对金钴混合粉在不同压力下低温高压扭转机械合金化过程中的剪切应力进行了测量。压力分别为5、8、10和12 GPa。Au-Co体系的特点是溶解度有限,组分性质不同。结果表明,与室温下的数据相比,在初始强度生长阶段和随后达到饱和阶段,剪切应力值都更高。随着低温机械合金化压力的增加,在加工的各个阶段都观察到抗剪切应变的相应增加。在这种情况下,在每个新的压力下,曲线的形状会发生变化,应变依赖性的阶段也会发生变化。这反映了非平衡合金的组织形成和相组成过程的极端异质性。x射线衍射图中反射最强烈的是基于金基基体的钴的过饱和fcc固溶体。同样由于机械合金化,系统的成分均匀地分布在合金的断口表面。
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Pressure dependence of shear stress during high-pressure torsion of the Au–Co alloys in liquid nitrogen
Measurements of the shear stress were carried out during mechanical alloying by high-pressure torsion of gold-cobalt powder mixing under cryogenic temperature at various pressures for the first time. The pressures were about 5, 8, 10 and 12 GPa. The Au–Co system is characterized by restricted solubility and difference in properties of the constituents. It was found that, in compari-son with the data obtained at room torsion temperature, the values of the shear stress are higher both at the stage of the initial intensive growth and subsequently, upon reaching saturation. With an in-crease in pressure of low-temperature mechanical alloying, a corresponding increase in the resistance to shear strain is observed at all stages of processing. In this case, the shape of the curves at each new pressure changes, as does the staging of the strain dependence. This reflects the extreme heter-ogeneity of the structure formation and phase composition processes of the non-equilibrium alloy. The most intense reflections in the X-ray diffractogram correspond to supersaturated fcc solid solu-tion of cobalt based on gold-base matrix. Also as a result of mechanical alloying, the components of the system are evenly distributed on the fracture surface of the alloy.
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