{"title":"热带木材短尾杉树茎的特征、植物化学和官能团分析","authors":"I. P. Udeozo, C. Ejikeme, A. Eboatu, H. Kelle","doi":"10.9734/acsj/2016/27047","DOIUrl":null,"url":null,"abstract":"The elucidation of Bombax brevicuspe wood was analysed for thermal and physico-chemical techniques. The results obtained were as follows: afterglow time 253.67 sec, flame duration 113.33 sec, flame propagation rate 20.3x10-2cm.s-1, ignition time 2.33 sec, thermal conductivity 51.34x102Umoh/cm, electrical conductivity 5.3x10-3Sm-1, ash content 3.4%, moisture content 29.97%, oven dry density 22.3x10-2g.cm-3, water imbibitions (at different time intervals: 30 mins 46.6%, 5hrs 87.6% and 24 hrs 148.9%), etc, These results showed it to be a good timber suitable for various construction purposes. The elemental analysis obtained through Atomic Absorption \nSpectrophotometer (AAS) indicated the absence of Ca, as well as the presence of Na, K, Pb, Mg, Zn, As, Cu, Hg and Cd in their decreasing order of magnitude respectively as follows: 1.07%, 0.08%, 0.08%, 0.07%, 0.05%, 0,02%, 0.01%, 0.01% and 0.003%. Thin Layer Chromatographic (TLC) analysis gave Retardation factor (Rf) value of 0.62 in the chloroform-methanol extract. The phytochemical screening showed the presence of all the tested secondary metabolites except steroids which indicated its therapeutic ability. Their proportions are indicated thus; saponins (10.2%), tannins (920 Mg/100 g), flavonoids (8.0%), carbohydrates (1.62 Mg/g), proteins (1.55%), glycosides (356 Mg/100 g) and alkaloids (5.6%). The Fourier Transform Infrared (FTIR) and Ultraviolet (UV) spectra suggested that the active compound might be 1,2,3-trisubstituted aromatic compound with C=O, O-H and C=N groups attached. The chemical components analysis showed the presence of cellulose 43%, hemicelluloses 20%, lignin 29% and other constituents in their right \nproportion. From the results, Bombax brevicuspe wood could be used for various construction purposes and it also poses some medicinal ability due to the presence of secondary metabolites","PeriodicalId":7399,"journal":{"name":"American Chemical Science Journal","volume":"5 1","pages":"1-8"},"PeriodicalIF":0.0000,"publicationDate":"2016-01-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Characterisation, Phytochemical and Functional Groups Assay of Bombax brevicuspe Stem: A Tropical Timber\",\"authors\":\"I. P. Udeozo, C. Ejikeme, A. Eboatu, H. Kelle\",\"doi\":\"10.9734/acsj/2016/27047\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The elucidation of Bombax brevicuspe wood was analysed for thermal and physico-chemical techniques. The results obtained were as follows: afterglow time 253.67 sec, flame duration 113.33 sec, flame propagation rate 20.3x10-2cm.s-1, ignition time 2.33 sec, thermal conductivity 51.34x102Umoh/cm, electrical conductivity 5.3x10-3Sm-1, ash content 3.4%, moisture content 29.97%, oven dry density 22.3x10-2g.cm-3, water imbibitions (at different time intervals: 30 mins 46.6%, 5hrs 87.6% and 24 hrs 148.9%), etc, These results showed it to be a good timber suitable for various construction purposes. The elemental analysis obtained through Atomic Absorption \\nSpectrophotometer (AAS) indicated the absence of Ca, as well as the presence of Na, K, Pb, Mg, Zn, As, Cu, Hg and Cd in their decreasing order of magnitude respectively as follows: 1.07%, 0.08%, 0.08%, 0.07%, 0.05%, 0,02%, 0.01%, 0.01% and 0.003%. Thin Layer Chromatographic (TLC) analysis gave Retardation factor (Rf) value of 0.62 in the chloroform-methanol extract. The phytochemical screening showed the presence of all the tested secondary metabolites except steroids which indicated its therapeutic ability. Their proportions are indicated thus; saponins (10.2%), tannins (920 Mg/100 g), flavonoids (8.0%), carbohydrates (1.62 Mg/g), proteins (1.55%), glycosides (356 Mg/100 g) and alkaloids (5.6%). The Fourier Transform Infrared (FTIR) and Ultraviolet (UV) spectra suggested that the active compound might be 1,2,3-trisubstituted aromatic compound with C=O, O-H and C=N groups attached. The chemical components analysis showed the presence of cellulose 43%, hemicelluloses 20%, lignin 29% and other constituents in their right \\nproportion. From the results, Bombax brevicuspe wood could be used for various construction purposes and it also poses some medicinal ability due to the presence of secondary metabolites\",\"PeriodicalId\":7399,\"journal\":{\"name\":\"American Chemical Science Journal\",\"volume\":\"5 1\",\"pages\":\"1-8\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2016-01-10\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"American Chemical Science Journal\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.9734/acsj/2016/27047\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"American Chemical Science Journal","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.9734/acsj/2016/27047","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
摘要
对短叶杉木材进行了热、理化分析。结果表明:余辉时间253.67秒,火焰持续时间113.33秒,火焰传播速率20.3x10-2cm。s-1,点火时间2.33秒,导热系数51.34x102Umoh/cm,电导率5.3x10-3Sm-1,灰分含量3.4%,含水率29.97%,烘箱干密度22.3x10-2g。吸水率(不同时间间隔:30 min 46.6%, 5h 87.6%, 24 h 148.9%)等,是一种适用于各种建筑用途的优良木材。原子吸收分光光度计(AAS)元素分析表明,Ca的存在率为1.07%、0.08%、0.08%、0.07%、0.07%、0.05%、0.02%、0.01%、0.01%、0.003%,Na、K、Pb、Mg、Zn、as、Cu、Hg、Cd的存在率依次为0.07%、0.08%、0.08%、0.07%、0.05%。薄层色谱(TLC)分析表明,氯仿-甲醇提取物的阻滞因子(Rf)值为0.62。植物化学筛选显示,除甾体外,所有被测次级代谢物均存在,表明其具有治疗能力。它们的比例是这样表示的;皂苷(10.2%)、单宁(920 Mg/100 g)、类黄酮(8.0%)、碳水化合物(1.62 Mg/g)、蛋白质(1.55%)、糖苷(356 Mg/100 g)和生物碱(5.6%)。傅里叶变换红外光谱(FTIR)和紫外光谱(UV)表明,活性化合物可能是由C=O、O- h和C=N基团连接的1,2,3-三取代芳香化合物。化学成分分析表明,纤维素占43%,半纤维素占20%,木质素占29%,其他成分按适当比例存在。综上所述,短叶杉木可用于多种建筑用途,且由于其次生代谢产物的存在,具有一定的药用价值
Characterisation, Phytochemical and Functional Groups Assay of Bombax brevicuspe Stem: A Tropical Timber
The elucidation of Bombax brevicuspe wood was analysed for thermal and physico-chemical techniques. The results obtained were as follows: afterglow time 253.67 sec, flame duration 113.33 sec, flame propagation rate 20.3x10-2cm.s-1, ignition time 2.33 sec, thermal conductivity 51.34x102Umoh/cm, electrical conductivity 5.3x10-3Sm-1, ash content 3.4%, moisture content 29.97%, oven dry density 22.3x10-2g.cm-3, water imbibitions (at different time intervals: 30 mins 46.6%, 5hrs 87.6% and 24 hrs 148.9%), etc, These results showed it to be a good timber suitable for various construction purposes. The elemental analysis obtained through Atomic Absorption
Spectrophotometer (AAS) indicated the absence of Ca, as well as the presence of Na, K, Pb, Mg, Zn, As, Cu, Hg and Cd in their decreasing order of magnitude respectively as follows: 1.07%, 0.08%, 0.08%, 0.07%, 0.05%, 0,02%, 0.01%, 0.01% and 0.003%. Thin Layer Chromatographic (TLC) analysis gave Retardation factor (Rf) value of 0.62 in the chloroform-methanol extract. The phytochemical screening showed the presence of all the tested secondary metabolites except steroids which indicated its therapeutic ability. Their proportions are indicated thus; saponins (10.2%), tannins (920 Mg/100 g), flavonoids (8.0%), carbohydrates (1.62 Mg/g), proteins (1.55%), glycosides (356 Mg/100 g) and alkaloids (5.6%). The Fourier Transform Infrared (FTIR) and Ultraviolet (UV) spectra suggested that the active compound might be 1,2,3-trisubstituted aromatic compound with C=O, O-H and C=N groups attached. The chemical components analysis showed the presence of cellulose 43%, hemicelluloses 20%, lignin 29% and other constituents in their right
proportion. From the results, Bombax brevicuspe wood could be used for various construction purposes and it also poses some medicinal ability due to the presence of secondary metabolites