用气相色谱-质谱分析方法测定了克罗地亚传统牛奶酪和山羊奶酪中挥发性化合物的含量

IF 0.5 Q4 CHEMISTRY, MULTIDISCIPLINARY Chemistry Journal of Moldova Pub Date : 2023-06-01 DOI:10.19261/cjm.2023.1076
Ani Radonis, M. Žekić
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引用次数: 0

摘要

在动物皮袋中成熟的奶酪属于传统奶酪,与它们的发源地国家的文化和历史密切相关。它们的主要特异性是在动物皮袋中厌氧成熟。本研究的目的是确定一袋由生牛奶或山羊奶制成的羊皮中克罗地亚奶酪的挥发性化合物,并将它们与这些传统奶酪的香气联系起来。采用顶空固相微萃取法(HS-SPME)和超声溶剂萃取法(USE)提取挥发物,气相色谱-质谱联用(GC-MS)分析挥发物。共鉴定出32种挥发物,其中羧酸类12种,酯类8种,醇类6种,酮类3种,烃类2种,醛类1种。HS-SPME法得到的样品中脂肪酸和醇含量最多,而USE法得到的样品中脂肪酸含量最多。
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Volatile compounds identified in traditional croatian cow’s and goat’s cheeses matured in lambskin sack determined by GC-MS analysis
Cheeses ripened in animal skin sacks belong to traditional cheeses that are strongly connected to the culture and history of the country from which they originate. Their main specificity is anaerobic ripening in an animal skin sack. The aim of this study was to determine the volatile compounds of Croatian cheeses in a sack of lamb skin produced from either raw cow’s or goat’s milk and relate them to the aroma of these traditional cheeses. Volatile compounds were extracted by headspace solid-phase microextraction (HS-SPME) and ultrasonic solvent extraction (USE) and analysed by gas chromatography-mass spectrometry (GC-MS). A total of 32 volatiles were identified in the cheese samples, including 12 carboxylic acids, 8 esters, 6 alcohols, 3 ketones, 2 hydrocarbons and 1 aldehyde. In the samples obtained by HS-SPME, the fatty acids and alcohols were the most abundant, while in the samples obtained by USE, the fatty acids were the most abundant.
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来源期刊
Chemistry Journal of Moldova
Chemistry Journal of Moldova CHEMISTRY, MULTIDISCIPLINARY-
CiteScore
0.90
自引率
20.00%
发文量
8
审稿时长
12 weeks
期刊介绍: "Chemistry Journal of Moldova. General, Industrial and Ecological Chemistry" seeks to publish experimental or theoretical research results of outstanding significance and timeliness in all fields of Chemistry, including Industrial and Ecological Chemistry. The main goal of this edition is strengthening the Chemical Society of Moldova, following development of research in Moldovan chemical institutions and promotion of their collaboration with international chemical community. Manuscripts are welcome from all countries.
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