静电纺LaMnO3纳米纤维的生长与表征

Y. Maung, Zin Min Myat, T. Win, K. Soe
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引用次数: 1

摘要

采用静电纺丝技术将PVA/[LaCl3+MnCl2+(NH4)2CO3]复合材料在600℃下煅烧,得到了LaMnO3纳米纤维的多晶钙钛矿结构。采用热重法和同步差热分析(TG-DTA)对样品的分解和结晶行为进行了研究。用x射线衍射(XRD)对晶体结构和相形成进行了表征。通过扫描电镜(SEM)计算了不同纺丝间隔下LaMnO3纳米纤维在600℃下的直径分别为42 nm和55 nm。对纤维的直径和形态进行了扫描电镜分析。
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Growth and Characterization of Electrospun LaMnO3 Nanofibers by Electrospinning Technique
The polycrystalline perovskite structure of LaMnO3 nanofibers was obtained by calcination of the PVA/[LaCl3+MnCl2+(NH4)2CO3] composite at 600°C with electrospinning technique. The decomposition and crystalline behavior of sample were examined by Thermogravimetric and Simultaneous Differential Thermal Analysis (TG-DTA). The crystal structure and phase formation were characterized by X-ray Diffraction (XRD). Scanning Electron Microscopy (SEM) was performed and the diameters of the LaMnO3 nanofibers were calculated to be 42 nm and 55 nm with different spinning intervals at 600°C. SEM analysis was also carried out to examine the fiber diameters and morphological properties.
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