分级结构高比表面积氧化铝在FeCrAl合金丝上的生长

Chandni Rallan, Aaron Akah, P. Hill, A. Garforth
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引用次数: 2

摘要

研究了在不同温度和时间周期下,由于商用FeCrAl合金丝(0.5 mm厚)氧化而形成的亚稳氧化铝相。使用热重分析仪(TGA)在空气中等温氧化样品。使用电子扫描电子显微镜(ESEM)分析氧化样品的形貌,使用能量色散x射线分析仪(EDX)对表面进行x射线分析。采用x射线衍射(XRD)技术对氧化产物的生长进行了表征。整个研究表明,在800°C以上等温氧化数小时后,在FeCrAl合金丝表面生长高表面积的γ氧化铝是可能的。
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Growth of Hierarchically Structured High-Surface Area Alumina on FeCrAl Alloy Wires
The formation of metastable alumina phases due to the oxidation of commercial FeCrAl alloy wires (0.5 mm thickness) at various temperatures and time periods has been examined. Samples were isothermally oxidised in air using a thermogravimetric analyzer (TGA). The morphology of the oxidised samples was analyzed using an Electronic Scanning Electron Microscope (ESEM) and X-ray on the surface analysis was done using an Energy Dispersive X-Ray (EDX) analyzer. The technique of X-Ray Diffraction (XRD) was used to characterize the phase of the oxide growth. The entire study showed that it was possible to grow high-surface area gamma alumina on the FeCrAl alloy wire surfaces when isothermally oxidised above 800°C over several hours.
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