利用原春草水萃取物绿色合成纳米银颗粒

M. M. Nadzir, F. N. Idris, Khairunisa Hat
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引用次数: 8

摘要

纳米粒子的需求正在增加,特别是在化妆品、生物医学科学、环境卫生和药物输送等领域,这主要是由于其微小的颗粒尺寸。原丘bens (G. procumbens)是一种在东南亚很容易找到的药用植物,可以用来合成银纳米粒子(AgNPs),而不需要任何刺激性和有毒的化学物质。以原藜叶提取物为原料合成AgNPs,考察硝酸银的浓度、植物提取物(PE)的浓度、反应时间和PE与硝酸银的比例对AgNPs合成的影响。将硝酸银与聚乙烯混合制备银纳米粒子,并用紫外可见光谱(UV-Vis)、傅里叶变换红外光谱(FTIR)、透射电子显微镜(TEM)和zeta电位分析对合成的银纳米粒子进行了表征。研究发现,原豆叶提取物能够降低水中银离子,导致银离子的颜色变化,表明银纳米粒子的形成。紫外可见光谱显示表面等离子体共振峰强度在449 ~ 471 nm之间。Zeta电位分析证明了AgNPs的稳定性,其值为- 40 mV。FTIR分析表明AgNPs被各种蛋白质分子覆盖,TEM证实了纳米颗粒的球形。结果表明,原甘草是合成AgNPs的潜在天然来源。纳米粒子的需求正在增加,特别是在化妆品、生物医学科学、环境卫生和药物输送等领域,这主要是由于其微小的颗粒尺寸。原丘bens (G. procumbens)是一种在东南亚很容易找到的药用植物,可以用来合成银纳米粒子(AgNPs),而不需要任何刺激性和有毒的化学物质。以原藜叶提取物为原料合成AgNPs,考察硝酸银的浓度、植物提取物(PE)的浓度、反应时间和PE与硝酸银的比例对AgNPs合成的影响。将硝酸银与聚乙烯混合制备银纳米粒子,并用紫外可见光谱(UV-Vis)、傅里叶变换红外光谱(FTIR)、透射电子显微镜(TEM)和zeta电位分析对合成的银纳米粒子进行了表征。研究发现,原丘叶提取物能降低水银离子,使原丘叶的颜色发生变化。
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Green synthesis of silver nanoparticle using Gynura procumbens aqueous extracts
Nanoparticle is increasing in demand especially in the area such as cosmetics, biomedical sciences, environmental health and drug delivery which mainly due to its minute particle size. Gynura procumbens (G. procumbens) is a medicinal plant that easily found in Southeast Asia and can be used to synthesize silver nanoparticles (AgNPs) without any harsh and toxic chemicals. The objectives of this study were to synthesis AgNPs using G. procumbens leaves extract and investigate the effect of concentration of silver nitrate, concentration of plant extract (PE), reaction time and ratio of PE to silver nitrate in synthesizing AgNPs. Silver nanoparticles were prepared by mixing silver nitrate with PE and the synthesized AgNPs were characterized by UV-Vis spectroscopy, Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), and zeta potential analysis. It was discovered that G. procumbens leaves extract able to reduce aqueous silver ions which resulted in a colour change indicating AgNPs formation. The UV-Vis spectrum showed surface plasmon resonance peak intensity ranging from 449 to 471 nm. Zeta potential analysis proved stability of AgNPs by having the value −40 mV. The FTIR analysis showed that AgNPs were capped by various protein molecules and TEM confirmed the spherical shape of nanoparticles. The data compiled illustrated that G. procumbens is a potential natural source for synthesizing AgNPs.Nanoparticle is increasing in demand especially in the area such as cosmetics, biomedical sciences, environmental health and drug delivery which mainly due to its minute particle size. Gynura procumbens (G. procumbens) is a medicinal plant that easily found in Southeast Asia and can be used to synthesize silver nanoparticles (AgNPs) without any harsh and toxic chemicals. The objectives of this study were to synthesis AgNPs using G. procumbens leaves extract and investigate the effect of concentration of silver nitrate, concentration of plant extract (PE), reaction time and ratio of PE to silver nitrate in synthesizing AgNPs. Silver nanoparticles were prepared by mixing silver nitrate with PE and the synthesized AgNPs were characterized by UV-Vis spectroscopy, Fourier transform infrared spectroscopy (FTIR), transmission electron microscopy (TEM), and zeta potential analysis. It was discovered that G. procumbens leaves extract able to reduce aqueous silver ions which resulted in a colour change indicating A...
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