硫酸法酸浓度和时间对合成金红石废合成二氧化钛的影响

Ahmad Mukifza, S. Yusof, Clarence M. Ongkudon, Eddy M. Farid, Huzaikha Binti Awang
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引用次数: 1

摘要

提出了一种快速简便的制备二氧化钛(TiO2)的方法,即在苛性水热分解的条件下,再以硫酸(H2SO4)为原料进行硫酸盐处理。以金红石废渣为起始原料,经过这两种简单工艺,研究了硫酸盐工艺中酸浓度和时间的影响。用电子色散(EDX)表征产物的化学成分,并用场发射扫描电镜(FESEM)分析产物的显微照片。本研究表明,在中等酸浓度、1M ~ 3M、较短处理时间、3h ~ 5h的硫酸盐工艺条件下,成功合成了二氧化钛(TiO2)。
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Effect of acid concentration and time of sulphate process on synthesizing the titanium dioxide from synthetic rutile waste
A fast and easy method for preparing the titanium dioxide (TiO2), using a caustic hydrothermal decomposition conditions followed with sulphate process using sulfuric acid (H2SO4), is presented. Synthetic rutile waste as a starting raw material going through these two simple processes then the effects of acid concentration and time of sulphate process were studied. The chemical composition of the product will be characterized using Electron Dispersive (EDX) and the micrographs were analyzed using a Field Emission Scanning Electron Microscope (FESEM). This study shows that a titanium dioxide (TiO2) was successfully synthesized after treated with medium acid concentration, 1M to 3M and short treatment time, 3h to 5h sulphate process.
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