水热法制备CdS-Zn3(PO4)2纳米复合材料及表征

G. Sridevi, S. Bhagade, V. Jayalakshmi, Sandhya Cole
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引用次数: 5

摘要

采用有效水热法制备了硫化镉磷酸锌(CdS-Zn3(PO4)2)纳米复合材料。水热技术可以在较低的反应温度下产生高度均匀的结晶产物并控制颗粒形态。采用粉末x射线衍射仪(XRD)、扩散反射分光光度计(DRS)、扫描电镜(SEM)对制备的粉末样品进行了表征。XRD技术表明,制备的CdS-Zn3(Po4)2纳米复合材料的平均晶粒尺寸在12 nm左右。通过XRD研究计算了应变和位错密度。用扫描电镜分析了样品的表面形貌。用扩散电子分光光度计根据Kubelka-Munk模型计算带隙能。
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Synthesis and characterization of CdS-Zn3(PO4)2 nanocomposite via hydrothermal method
Cadmium sulfide zinc phosphate (CdS-Zn3(PO4)2) nanocomposite is synthesized by effective hydrothermal method. Hydrothermal technique produces highly homogeneous crystalline product and controls particle morphology at low reaction temperatures. The prepared powder samples are characterized by Powder X-ray diffraction (XRD), Diffusion reflectance spectrophotometer (DRS), Scanning electron microscope (SEM). From XRD technique the average crystal size of prepared CdS-Zn3(Po4)2 nanocomposite is in the range of 12 nm. Strain and dislocation density are calculated from XRD studies. Surface morphology of the samples are analyzed by SEM. Bandgap energies are calculated from Kubelka-Munk model by Diffusion electron spectrophotometer.
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