水热生长纳米结构金属二氧化钛的物理性质

M. Zakaria, N. Farahin, R. Osman, Sh. Nadzirah, A. H. Azman, U. Hashim, M. K. Md Arshad
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引用次数: 0

摘要

采用水热法在TiO2种子层上研究了二氧化钛(TiO2)纳米线的生长。本文采用两步法在Si(100)衬底上生长纳米线TiO2。采用溶胶-凝胶法制备不同的TiO2种子层,经自旋包覆和退火沉积,然后采用水热法制备TiO2纳米线。以乙酸为稳定剂合成TiO2种子层。本研究的目的是了解薄膜上的多晶尺寸对作为表面声波(SAW)生物传感器传感区域的纳米线直径的作用。采用x射线衍射(XRD)、扫描电镜(SEM)、场发射扫描电镜(FESEM)和原子力显微镜(AFM)对薄膜种子层和TiO2纳米线的形貌和微观结构进行了表征。
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Physical properties of hydrothermal growth nanostructure metal titanium dioxide
Growth of titanium dioxide (TiO2) nanowires was studied on the seed layer of TiO2 through hydrothermal growth method. Here, the growth of nanowires TiO2 on Si (100) substrates by using the two steps method. Different seed layers of TiO2 were prepared by using sol-gel method, deposited by spin coating and annealing, followed by the growth of TiO2 nanowires by using the hydrothermal method. Acetic acid was used as a stabilizer to synthesize a TiO2 seed layer. The aim of this study was to understand the role of polycrystalline size on thin film towards the diameter of nanowires grown as a sensing area in Surface Acoustic Wave (SAW) Biosensor. The morphology and microstructure of the thin film seed layer and TiO2 nanowires were characterized using X-Ray diffraction (XRD), scanning electron microscope (SEM), field emission scanning electron microscope (FESEM) and atomic force microscopy (AFM).
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