生物场能量处理2,4-二羟基二苯甲酮的物理、热及光谱性质

M. Trivedi, R. M. Tallapragada, A. Branton, Dahryn Trivedi, G. Nayak, R. Mishra, S. Jana
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引用次数: 4

摘要

研究背景:2,4-二羟基二苯甲酮(DHBP)是一种用于合成药物制剂的有机化合物。本研究的目的是研究生物场能量处理对DHBP的物理、热和光谱特性的影响。研究分为两组(对照组和实验组)。对照组保持不治疗,治疗组接受特里维迪的生物场能量治疗。方法:采用x射线衍射(XRD)、差示扫描量热法(DSC)、热重分析(TGA)、激光粒度分析仪、比表面积分析仪、傅里叶变换红外光谱(FT-IR)和紫外可见光谱(UV-vis)对对照和处理后的DHBP样品进行表征。结果:XRD研究表明,与对照样品相比,处理后的DHBP的单位细胞体积和分子量略有下降。然而,XRD研究表明,处理后的DHBP的平均晶粒尺寸比对照样品增加了32.73%。DSC表征表明,处理后样品的熔化温度没有明显变化。与对照组相比,处理后的DHBP融合潜热显著增加11.67%。然而,TGA分析表明,处理后的DHBP的最高热分解温度(Tmax)为257.66oC,较对照样品(260.93oC)有所降低。粒径分析表明,处理后的DHBP的粒径(d50和d99)比对照样品增加了41%和15.8%。此外,表面积分析显示,处理过的DHBP的表面积减少了9.5%,这与粒径结果相一致。然而,FT-IR分析显示,与对照组相比,处理后的样品中甲基拉伸向下移动(2885→2835 cm-1)。紫外光谱分析表明,与对照相比,处理后样品(T1)的吸收峰蓝移323→318 nm。结论:与对照组相比,处理后的DHBP在物理、热、光谱等方面均有显著变化。
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Physical, Thermal and Spectral Properties of Biofield Energy Treated 2,4-Dihydroxybenzophenone
Study background: 2,4-Dihydroxybenzophenone (DHBP) is an organic compound used for the synthesis of pharmaceutical agents. The objective of this study was to investigate the influence of biofield energy treatment on the physical, thermal and spectral properties of DHBP. The study was performed in two groups (control and treated). The control group remained as untreated, and the treated group received Mr. Trivedi’s biofield energy treatment. Methods: The control and treated DHBP samples were further characterized by X-ray diffraction (XRD), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), laser particle size analyser, surface area analyser, Fourier transform infrared (FT-IR) spectroscopy, and ultra violet-visible spectroscopy (UV-vis) analysis. Results: The XRD study indicated a slight decrease in the volume of the unit cell and molecular weight of treated DHBP as compared to the control sample. However, XRD study revealed an increase in average crystallite size of the treated DHBP by 32.73% as compared to the control sample. The DSC characterization showed no significant change in the melting temperature of treated sample. The latent heat of fusion of the treated DHBP was substantially increased by 11.67% as compared to the control. However, TGA analysis showed a decrease in the maximum thermal decomposition temperature (Tmax) of the treated DHBP (257.66oC) as compared to the control sample (260.93oC). The particle size analysis showed a substantial increase in particle size (d50 and d99) of the treated DHBP by 41% and 15.8% as compared to the control sample. Additionally, the surface area analysis showed a decrease in surface area by 9.5% in the treated DHBP, which was supported by the particle size results. Nevertheless, FT-IR analysis showed a downward shift of methyl group stretch (2885→2835 cm-1) in the treated sample as compared to the control. The UV analysis showed a blue shift of absorption peak 323→318 nm in the treated sample (T1) as compared to the control. Conclusion: Altogether, the results showed significant changes in the physical, thermal and spectral properties of treated DHBP as compared to the control.
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