ECAP加工温度对商品纯铜微观组织、织构演变及力学性能的影响

A. I. Alateyah
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The enhancement of various metals strength such as copper can be reached by heat treatment and the addition of other alloying elements. However, this technique can lower the ductility and electric conductivity [4]. The other successful way is by improving the structure to obtain ultrafine-grained (UFG) and a large grain boundary area [5,6]. These outcomes can be reached by undertaken severe plastic deformation method (SDP) [613]. Severe plastic deformation technique has been used widely nowadays due to their influence on the microstructure behavior. The production of ultrafinegrained microstructures and the deformation of metallic and alloy materials can be achieved by this process. 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As a In this study, the severe plastic deformation (SPD) behavior of commercial-grade pure copper processed using equal channel angular pressing (ECAP) was investigated. The copper rods were processed for up to 4 passes, both at room temperature and 200 C. The microstructure and texture evolution were studied using a field emission scanning electron microscope (FESEM) equipped with an electron back scattered (EBSD) detector. The effect of ECAP processing on the tensile properties, micro-hardness, and impact toughness was studied. After 1 pass, the average grain size of the rods was determined to be 2.694 and 3.9066 μm at room temperature and 200 C, respectively. In addition, after 4 passes through ECAP, the strength of the ECAPed samples increased to 381 MPa, and 330 MPa at room temperature and 200 C, respectively; and the Vickers’ micro-hardness at the peripheral areas increased to 158, and 126, respectively. 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引用次数: 0

摘要

在过去十年中,工业对具有高强度和导电性的材料的大量需求正在广泛进行。几种类型的金属,包括银、铜、金和铝,由于它们的导电性水平而被大量利用。在成本比较方面,铝和铜是最合理的价格,具有这种导电性的优势。然而,由于两个原因,与其他金属相比,这些材料的导电性较低。第一个,杂质通过晶格的热振动放大电子散射。第二,包含晶界和位错的结构缺陷的出现[1-3]。平衡这一问题的能力是通过获得纯材料和提高机械强度。可以通过热处理和添加其他合金元素来提高铜等各种金属的强度。然而,这种技术会降低延展性和导电性[4]。另一种成功的方法是通过改进结构获得超细晶(UFG)和大晶界面积[5,6]。这些结果可以通过承受剧烈塑性变形法(SDP)达到[613]。剧烈塑性变形技术由于其对材料微观组织行为的影响而得到了广泛的应用。超细晶组织的产生以及金属和合金材料的变形可以通过该工艺实现。(SDP)最适用的工艺是等通道角挤压(ECAP),因为它可以高效地制造不同类型的超细晶材料[14-20],生产纳米晶块体材料[21],改善机械和物理性能[5],实现块体材料的均匀变形[22,23],处理金属流动力学和微观组织演变[20]。此外,利用ECAP可以增强材料的延展性,因为在不牺牲材料强度的情况下,纳米级晶粒尺寸与微米级或UFG相结合形成的双相微观结构得到增强[24]。ECAP方法可以利用各种形状的样品,如矩形,方形或圆形。通过在整个模具中无限次的道次,在此过程中可以获得组织的剧烈剪切变形,而尺寸不会发生剧烈变化。在本研究中,研究了商品级纯铜在等通道角挤压(ECAP)下的严重塑性变形(SPD)行为。采用场发射扫描电镜(FESEM)和电子背散射(EBSD)探测器研究了铜棒的显微组织和织构演变。研究了ECAP处理对拉伸性能、显微硬度和冲击韧性的影响。经过1次热处理,在室温和200℃下,晶粒尺寸分别为2.694和3.9066 μm。另外,经过4次ECAP后,ECAP样品在室温和200℃下的强度分别提高到381 MPa和330 MPa;外围区维氏硬度分别提高到158和126。另一方面,实验结果表明,ECAP通过次数对冲击能的影响不显著。
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On the Effect of ECAP Processing Temperature on the Microstructure, Texture Evolution and Mechanical Properties of Commercial Pure Copper
In the last decade, a large demand of the industries for a material with high level of strength and conductivity is widely undergoing. Several types of metals which includes, silver, copper, gold and aluminum are largely utilized due to their level of electrical conductivity. In term of cost comparison, the aluminum and copper are the most reasonable price with the advantage of this conductivity. However, these materials have lower electrical conductivity with compared to other metals due to two reasons. The first one, the impurities that enlarge the electron scattering by thermal vibrations of the crystal lattice. The second one, the attendance of structural imperfections which contain grain boundaries and dislocations [1-3]. The Ability of balancing this issue is via obtaining of the both pure materials with improvement of mechanical strength. The enhancement of various metals strength such as copper can be reached by heat treatment and the addition of other alloying elements. However, this technique can lower the ductility and electric conductivity [4]. The other successful way is by improving the structure to obtain ultrafine-grained (UFG) and a large grain boundary area [5,6]. These outcomes can be reached by undertaken severe plastic deformation method (SDP) [613]. Severe plastic deformation technique has been used widely nowadays due to their influence on the microstructure behavior. The production of ultrafinegrained microstructures and the deformation of metallic and alloy materials can be achieved by this process. The most applicable processes of the (SDP) is equalchannel angular pressing (ECAP) due to their highly effective of fabricating different types of ultrafine-grained materials [14-20], producing nano-crystalline bulk materials [21], improving both mechanical and physical properties [5], achieving the homogenously deformation of bulk material [22,23] and the dealing with the mechanics of metal flow and the microstructural evolution [20]. Furthermore, the ductility of material can be enhanced by utilizing ECAP, since the enhancement of a duplex microstructure shaped by nanometric grains sized coupled with micrometric or UFG without sacrificing the martials strength [24]. The ECAP method can utilized various sample's shape such as rectangular, square, or circular. By unlimited number of passes throughout the die, the severe shear deformation of microstructure can be obtained during this way without dramatic changes in the dimensions. As a In this study, the severe plastic deformation (SPD) behavior of commercial-grade pure copper processed using equal channel angular pressing (ECAP) was investigated. The copper rods were processed for up to 4 passes, both at room temperature and 200 C. The microstructure and texture evolution were studied using a field emission scanning electron microscope (FESEM) equipped with an electron back scattered (EBSD) detector. The effect of ECAP processing on the tensile properties, micro-hardness, and impact toughness was studied. After 1 pass, the average grain size of the rods was determined to be 2.694 and 3.9066 μm at room temperature and 200 C, respectively. In addition, after 4 passes through ECAP, the strength of the ECAPed samples increased to 381 MPa, and 330 MPa at room temperature and 200 C, respectively; and the Vickers’ micro-hardness at the peripheral areas increased to 158, and 126, respectively. In the other hand, the experimental findings revealed that the number of ECAP passes has insignificant effect on the impact energy.
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