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Insights into the Emerging Collagen-based Bio-ink in 3D Bio-printing for Tissue Engineering: A Short Review 洞察三维生物打印技术中用于组织工程的新兴胶原基生物墨水:简评
Pub Date : 2024-07-01 DOI: 10.5185/amlett.2024.031754
Sahariya Priya, Sakar Mohan, A. Murali, R. Ramesh, Sung Soo Han
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引用次数: 0
A Review on Synthesis Methods of Materials Science and Nanotechnology 材料科学与纳米技术合成方法综述
Pub Date : 2024-07-01 DOI: 10.5185/amlett.2024.031758
Avadhesh Yadav
Materials science is a fast developing field of research in which a lot of advancements have been reported in few decades. The progress in materials science is essential due to its wide range of applications in solid state fuel cells, display materials, solar cells, energy storage devices, automotive sectors, electronics and environment, mechanical, medical & aerospace industries. Doping and substitutions in host materials are excellent ways of changing the properties of any materials. There are two main forms of materials, thin film and bulk, which are used in research. These two forms of materials are synthesized by two basic approaches, named as top-down and bottom-up. Bottom-up and top-down approaches are comprised of several synthesis methods, e.g., solid state reaction method, hydrothermal method, co-precipitation method, sol gel method, auto-combustion method, melt quench method, evaporation method, sputtering method, pulse laser deposition method, spin coating method and spray pyrolysis method. Each synthesis method has its unique procedure as well as merits and demerits. The solid state reaction route is one of the simplest synthesis method, which requires heating of the materials which were grounded for homogeneous mixing of the various oxide ingredients. The bulk and thin films at low reaction temperatures were prepared by sol-gel synthesis route which provides the high purity products. Co-precipitation method provides homogenous particle size which is a very energy efficient method. Thus, the synthesis method is an essential factor for materials science and nanotechnology research. The present article is an attempt to review the synthesis methods and their merits or demerits.
材料科学是一个快速发展的研究领域,几十年来取得了许多进展。由于材料科学在固态燃料电池、显示材料、太阳能电池、储能设备、汽车行业、电子和环境、机械、医疗和航空航天工业中的广泛应用,材料科学的进步至关重要。在主材料中进行掺杂和替代是改变任何材料特性的绝佳方法。用于研究的材料主要有两种形式:薄膜和块状。这两种形式的材料通过两种基本方法合成,即自上而下和自下而上。自下而上和自上而下的方法包括多种合成方法,如固态反应法、水热法、共沉淀法、溶胶凝胶法、自燃法、熔淬法、蒸发法、溅射法、脉冲激光沉积法、旋镀法和喷雾热解法。每种合成方法都有其独特的程序和优缺点。固态反应路线是最简单的合成方法之一,它需要加热研磨好的材料,使各种氧化物成分均匀混合。通过溶胶-凝胶合成路线,可以在低反应温度下制备出高纯度的块状和薄膜。共沉淀法提供了均匀的粒度,是一种非常节能的方法。因此,合成方法是材料科学和纳米技术研究的重要因素。本文试图综述各种合成方法及其优缺点。
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引用次数: 0
Influence of Fiber Orientation on the Strength Properties of Paper-Epoxy Composites 纤维方向对纸-环氧树脂复合材料强度特性的影响
Pub Date : 2024-07-01 DOI: 10.5185/amlett.2024.031756
C. Helbrecht, R. Götzinger, S. Schabel
An important advantage of paper composites is their sustainability. Natural fibers store CO 2 during growth, they are recyclable and may be safely thermally recycled. In this work, composites out of laboratory paper and epoxy resin are generated in a hand lay-up process. The laboratory paper varies in the degree of fiber orientation. As a comparison, paper with isotropic fiber orientation is also used. The tensile strength for the isotropic paper composite is about 120 MPa. It can be observed that the tensile strength of the composite tends to increase with the increase of fiber orientation in the paper. The measured tensile strength of the oriented paper composites in the fiber direction is about 150 MPa and in cross fiber direction about 50 MPa. The strength characteristics are comparatively lower than for carbon or glass fiber reinforced composites, but the density of the paper composites investigated here is only about 1.26 g/cm 3 and the raw material price is significantly lower making paper composites economically attractive. At the end, strength values are modeled with the rule of mixture as well as with Kröling's strength model. In conclusion, tensile strength of oriented paper composites are higher than of isotropic paper.
纸张复合材料的一个重要优势是其可持续性。天然纤维在生长过程中会储存二氧化碳,可回收利用,并可安全地进行热回收。在这项工作中,通过手工铺层工艺生成了由实验纸和环氧树脂制成的复合材料。实验纸的纤维取向程度各不相同。作为对比,还使用了纤维取向各向同性的纸张。各向同性纸复合材料的拉伸强度约为 120 兆帕。可以看出,复合材料的抗拉强度随着纸张纤维取向的增加而增加。测得的取向纸复合材料在纤维方向上的抗拉强度约为 150 兆帕,在纤维交叉方向上的抗拉强度约为 50 兆帕。强度特性相对低于碳纤维或玻璃纤维增强复合材料,但此处研究的纸复合材料密度仅约为 1.26 g/cm 3,原材料价格明显较低,因此纸复合材料具有经济吸引力。最后,强度值是根据混合法则和克罗林强度模型得出的。总之,定向纸复合材料的抗拉强度高于各向同性纸。
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引用次数: 0
Influence of CNT Concentrations on Structural and Morphological Properties of PANI-SnO2-CNT Nanocomposite Thin Films and the Sensitivity Performance to Detect E. coli in Water 碳纳米管浓度对 PANI-SnO2-CNT 纳米复合薄膜的结构和形态特性以及检测水中大肠杆菌灵敏度性能的影响
Pub Date : 2024-07-01 DOI: 10.5185/amlett.2024.031757
Huda Abdullah, N. Naim, Mohamad Aiman Arif Omar, Jian Kang, Iskandar Yahya, N. Kamal, N. Aziz, Atiqah Afdzaluddin, Noraziah Zin, Mohd Hafiz Dzarfan Othman, Wing Yap
Carbon nanotubes (CNTs) are particularly attractive for use in sensors for environmental and health monitoring. This study proposes a new approach in developing polymer-metal-based sensor for E. coli detection by using CNTs incorporation. PANI-SnO 2 nanocomposite thin films were combined with CNTs to be fabricated as biosensing devices. PANI-(SnO 2 ) 1-x -CNT x nanocomposite thin films were synthesized using sol-gel method and deposited on a glass substrate by spin coating technique. The prepared thin films were characterized by X-ray diffraction (XRD), field scanning electron microscopy (FESEM), atomic field microscopy (AFM) and ultraviolet-visible (UV-vis) spectroscopy. The sensitivity performance of PANI-(SnO 2 ) 1-x -CNT x nanocomposite thin films were conducted by using current-voltage ( I-V ) measurements. From the results, XRD patterns show the appearance of PANI, SnO 2 and C peaks and the increasing crystallite size with the increasing of CNT concentration. FESEM images show the spherical shape of SnO 2 and the nanotubes of carbon in the diameter size range 30 – 100 nm and 150 – 220 nm respectively. AFM analysis has found out the roughness parameter has increased when CNT percentage was increased. The peaks from UV-Vis absorbance bands indicated the presence of CNT and SnO 2 at wavelength 270 nm and 370 nm respectively. From I-V measurement of the sensor, PANI-(SnO 2 ) 1-x -CNT x with x = 0.03 performed the highest sensitivity which is 16.32%. The results demonstrate that the increasing of CNT concentrations was increasing the sensitivity of PANI-(SnO 2 ) 1-x -CNT x thin films towards E. coli .
碳纳米管(CNT)在环境和健康监测传感器中的应用尤其具有吸引力。本研究提出了一种利用 CNTs 开发基于聚合物-金属的大肠杆菌检测传感器的新方法。将 PANI-SnO 2 纳米复合薄膜与 CNTs 结合,制成生物传感设备。采用溶胶-凝胶法合成了 PANI-(SnO 2 ) 1-x -CNT x 纳米复合薄膜,并通过旋涂技术沉积在玻璃基底上。利用 X 射线衍射 (XRD)、场扫描电子显微镜 (FESEM)、原子场显微镜 (AFM) 和紫外-可见 (UV-vis) 光谱对制备的薄膜进行了表征。通过电流-电压(I-V)测量,研究了 PANI-(SnO 2 ) 1-x -CNT x 纳米复合薄膜的灵敏度性能。从结果来看,XRD 图谱显示出现了 PANI、SnO 2 和 C 峰,并且随着 CNT 浓度的增加,结晶尺寸也在增大。FESEM 图像显示 SnO 2 呈球形,碳纳米管直径范围分别为 30 - 100 nm 和 150 - 220 nm。原子力显微镜分析发现,当碳纳米管比例增加时,粗糙度参数也随之增加。紫外-可见吸收带的峰值表明,在波长 270 纳米和 370 纳米处分别存在碳纳米管和氧化锡 2。从传感器的 I-V 测量结果来看,PANI-(SnO 2 ) 1-x -CNT x(x = 0.03)的灵敏度最高,达到 16.32%。结果表明,随着 CNT 浓度的增加,PANI-(SnO 2 ) 1-x -CNT x 薄膜对大肠杆菌的灵敏度也在增加。
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引用次数: 0
Chemical Processing and Physical-Chemical and Mechanical Characterizations of Poly (L-co-D, L lactic acid)/Polyethylene Glycol Mixtures for Application as a Biomedical Device 用作生物医学设备的聚(左旋-右旋乳酸)/聚乙二醇混合物的化学处理及物理化学和机械特性分析
Pub Date : 2024-07-01 DOI: 10.5185/amlett.2024.031755
V. Amaral, Juliana Souza, Thais Alves, F. Batain, Kessi Crescencio, Daniel Komatsu, Marco Chaud
The chemical processing of polymeric mixtures is a promising alternative for designing materials with new characteristics for biomedical applications. This work proposed to produce and characterize polymeric mixtures obtained using polyethylene glycol (PEG400 or PEG4000) with poly (L-co-D, L lactic acid)/PLDLA for biomedical use. The mixtures were prepared by the casting method. Characterizations were performed by Fourier transform infrared spectroscopy (FTIR), differential scanning calorimetry (DSC), mechanical properties (perforation, resilience, elastic modulus, plastic deformation, tensile strength and mucoadhesion) and in vitro biodisintegration studies. The results obtained by FTIR and DSC suggest that the chemical interactions that generate the mixtures between the polymers occurred through hydrogen bonds and/or dipole-dipole interactions. Chemical interactions created compounds that were more hydrophilic and had different rearrangements when using PEG400 or PEG4000 in the mixture. The mechanical tests showed changes in the resistance of the materials, highlighting the exponential value of plastic deformation of PLDLA/PEG400, significantly increasing the plasticity of this structure by 111-fold about PLDLA/PEG4000. In the biodisintegration study, after 120 hours, greater mass loss was observed for PLDLA/PEG4000 (68.82 ± 1.46%). Hydrolytic disintegration did not influence pH values, which remained between 7.34 and 7.41 during the study. In conclusion, these mixtures can provide valuable characteristics to produce a biocompatible biomedical device with properties to support tissue regeneration, where the issue of plastic deformation is necessary in collaboration with the formation of pores, after PEG dissolution in vivo .
对聚合物混合物进行化学处理是为生物医学应用设计具有新特性的材料的一种有前途的替代方法。这项工作旨在生产聚乙二醇(PEG400 或 PEG4000)与聚(L-co-D,L 乳酸)/PLDLA 的聚合物混合物,并确定其生物医学用途的特性。混合物采用浇铸法制备。通过傅立叶变换红外光谱(FTIR)、差示扫描量热法(DSC)、机械性能(穿孔、回弹性、弹性模量、塑性变形、拉伸强度和粘附性)和体外生物降解研究进行了表征。傅立叶变换红外光谱和 DSC 得出的结果表明,产生聚合物混合物的化学作用是通过氢键和/或偶极-偶极相互作用进行的。在混合物中使用 PEG400 或 PEG4000 时,化学作用产生的化合物亲水性更强,重排方式也不同。机械测试表明,材料的抗性发生了变化,突出显示了 PLDLA/PEG400 的塑性变形指数值,这种结构的可塑性比 PLDLA/PEG4000 提高了 111 倍。在生物崩解研究中,120 小时后,观察到 PLDLA/PEG4000 的质量损失更大(68.82 ± 1.46%)。水解崩解不影响 pH 值,研究期间 pH 值保持在 7.34 和 7.41 之间。总之,这些混合物可为生产具有支持组织再生特性的生物相容性生物医学设备提供宝贵的特性,其中塑性变形问题与 PEG 在体内溶解后形成的孔隙是必要的。
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引用次数: 0
Exploring Nanocellulose-Based Materials for Energy Conversion and Storage Devices 探索用于能量转换和储存设备的纳米纤维素基材料
Pub Date : 2024-07-01 DOI: 10.5185/amlett.2024.031753
Nidhi Patel, Rahul Bairwan, H. P. S. Abdul Khalil, M. Ahmad, E. Yahya, Soni Thakur, Kanchan Jha
This review will provide a quick overview of the benefits and
本评论将简要介绍以下方面的益处和特点
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引用次数: 0
IAAM's Pledge for Global Climate Resilience at COP 28 国际建筑与城市规划学会在《公约》缔约方会议第二十八届会议上对全球气候复原力的承诺
Pub Date : 2024-04-01 DOI: 10.5185/amlett.2024.021745
Ashutosh Tiwari
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引用次数: 0
Comparative Study of the Photothermal Behavior of Polydopamine-, Polypyrrole-, and Carbon Nanotubes-based Materials 聚多巴胺、聚吡咯和碳纳米管基材料的光热行为比较研究
Pub Date : 2024-04-01 DOI: 10.5185/amlett.2024.021750
Gabriela Herrera Rodriguez, Andya Ramírez Irigoyen, Karla F García Verdugo, Ana Torres Figueroa, Brianda M Salazar Salas, José Encinas Encinas, Cinthia Jhovanna Pérez Martínez, Teresa del Castillo-Castro
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引用次数: 0
A Review on Bio-oil Upgradation by using Physico-chemical Methods 使用物理化学方法提升生物油等级综述
Pub Date : 2024-04-01 DOI: 10.5185/amlett.2024.021747
D. Bisen, Ashish Singh Chouhan
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引用次数: 0
A Study of the Structural, Optical and Antibacterial Properties of Green Synthesized Calcium Oxide Nanoparticles 绿色合成氧化钙纳米粒子的结构、光学和抗菌特性研究
Pub Date : 2024-04-01 DOI: 10.5185/amlett.2024.021749
Rekha S, Sreelakshmi P S, Akhila V S, Amrutha R, Anila E I
.
.
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引用次数: 0
期刊
Advanced Materials Letters
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