{"title":"席夫碱及乙二胺与1-苯基- 1,3 -丁二和4-氨基安替比林衍生的cr (Ii)、Fe (Ii)和Cd(Ii)配合物的合成与表征","authors":"Israa Jirjees","doi":"10.32792/utq/utj/vol14/1/7","DOIUrl":null,"url":null,"abstract":"Schiff base ligand [ (4Z,11aE,15E) -2,3,59,10 - pentamethyl -1,7,11-triphenyl-2,6,10,11,13,14-hexahydro -1H dipyrazol [4,3-b:3',4'-h][1,4,7,10] tetraazacyclotridecine ] was synthesized by reacting 1-Phenyl,1,3-butanedion and 4-aminoantipyrin with Ethylenediamine.Its complexes with Cr (II),Fe (II) and Cd (II) reaction of the metal salt with the ligand characterization ligands and its complexes were characterized by elements analyses , FT-IR , Mass techniques and 1 H-NMR","PeriodicalId":23465,"journal":{"name":"University of Thi-Qar Journal","volume":"49 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2019-04-25","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Synthesis and Characterization of Schiffbases Andcr (Ii), Fe (Ii) and Cd(Ii) Complexes Derived From Ethelene Diammine With 1-Phenyl-1, 3-Butanedion and 4-Aminoantipyrine\",\"authors\":\"Israa Jirjees\",\"doi\":\"10.32792/utq/utj/vol14/1/7\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Schiff base ligand [ (4Z,11aE,15E) -2,3,59,10 - pentamethyl -1,7,11-triphenyl-2,6,10,11,13,14-hexahydro -1H dipyrazol [4,3-b:3',4'-h][1,4,7,10] tetraazacyclotridecine ] was synthesized by reacting 1-Phenyl,1,3-butanedion and 4-aminoantipyrin with Ethylenediamine.Its complexes with Cr (II),Fe (II) and Cd (II) reaction of the metal salt with the ligand characterization ligands and its complexes were characterized by elements analyses , FT-IR , Mass techniques and 1 H-NMR\",\"PeriodicalId\":23465,\"journal\":{\"name\":\"University of Thi-Qar Journal\",\"volume\":\"49 1\",\"pages\":\"\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2019-04-25\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"University of Thi-Qar Journal\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.32792/utq/utj/vol14/1/7\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"University of Thi-Qar Journal","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.32792/utq/utj/vol14/1/7","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Synthesis and Characterization of Schiffbases Andcr (Ii), Fe (Ii) and Cd(Ii) Complexes Derived From Ethelene Diammine With 1-Phenyl-1, 3-Butanedion and 4-Aminoantipyrine
Schiff base ligand [ (4Z,11aE,15E) -2,3,59,10 - pentamethyl -1,7,11-triphenyl-2,6,10,11,13,14-hexahydro -1H dipyrazol [4,3-b:3',4'-h][1,4,7,10] tetraazacyclotridecine ] was synthesized by reacting 1-Phenyl,1,3-butanedion and 4-aminoantipyrin with Ethylenediamine.Its complexes with Cr (II),Fe (II) and Cd (II) reaction of the metal salt with the ligand characterization ligands and its complexes were characterized by elements analyses , FT-IR , Mass techniques and 1 H-NMR
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