埋弧焊烧结焊剂的XRD和DTA分析

Ajay Kumar, H. Singh, S. Maheshwari
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引用次数: 4

摘要

对发达的结块助熔剂中结晶相的结构和化学分析进行了独特的研究。将氧化物、卤化物、碳酸盐、硅酸盐和铁合金的混合物用于埋弧焊,研制了32种助焊剂。本文只关注了32种助焊剂中的10种,用x射线衍射(XRD)对它们进行了分析,以了解在850°C左右烧结过程中形成的不同类型的氧化物和金属中心氧化数的变化。为了了解温度对不同化合物相变和熔化的影响,从1000°C到1400°C进行了差热分析(DTA)。本研究的目的是了解埋弧焊过程中已开发的凝聚剂的离子含量(百分比)和熔化行为。
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XRD and DTA Analysis of Developed Agglomerated Fluxes for Submerged Arc Welding
A unique study of structural and chemical analysis of crystalline phases in developed agglomerated fluxes was carried out. Thirty-two fluxes were developed by using a mixture of oxides, halides, carbonates, silicates, and ferroalloys for submerged arc welding. The present paper focuses on only ten (out of thirty-two) fluxes which were analyzed by X-ray diffraction (XRD) to know the different types of oxides formed and changed in oxidation number of metallic centers after sintering process at around 850∘C. To know the effect of temperature over phase transformation and melting of different compounds, differential thermal analysis (DTA) was carried out from 1000 to 1400∘C. This study aims to know the quantity of ions present (percentage) and melting behavior of developed agglomerated fluxes for submerged arc welding process.
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