抗结核候选物铁(III) 4-氟- n′-[(吡啶-4-基)羰基]苯并肼配合物的表征与合成

R. Ruswanto
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引用次数: 2

摘要

Fe (III)与4-氟- n′-[(吡啶-4-酰基)羰基]苯并肼配体的配合物的合成旨在找出其合成方法、配合物及所形成配合物的特征化合物配方。使用的仪器有紫外可见分光光度法、红外分光光度法和原子吸收分光光度法。Fe (III) 4-氟- n′-[(吡啶-4-酰基)羰基]苯并肼配合物的合成可以在78℃的温度下将溶解在乙醇中的金属与配体混合合成。合成的化合物可形成式为Fe(C13H10FN3O2)Cl3.2H2O的配合物。Fe (III) 4-氟- n′-[(吡啶-4-酰基)羰基]苯并肼配合物的最大波长为265.6 nm。540.0 cm-1红外光谱上官能团的吸收。关键词:合成,配合物,铁(III),苯并肼
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CHARACTERIZATION AND SYNTHESIZE OF Fe(III) 4-FLUORO-N’-[(PYRIDINE-4-YL)CARBONYL]BENZOHYDRAZIDE COMPLEX AS ANTITUBERCULOSIS CANDIDATE

Synthesis of Fe (III) complex compounds with 4-fluoro-N '- [(pyridine-4-yl) carbonyl] benzohydrazide ligand aims to find out the synthesis method, the complex and characteristic compound formulas of the complexes formed. Instruments used are UV-Visible Spectrophotometry, Infrared Spectrophotometry and Atomic Absorption Spectrophotometry. The synthesis of Fe (III) 4-fluoro-N '- [(pyridine-4-yl) carbonyl] benzohydrazide complexes can be synthesized by mixing metals and ligands dissolved in ethanol by heating at a temperature of 78oC. Compounds of synthesis can form complexes with the formula Fe(C13H10FN3O2)Cl3.2H2O. Characteristics of the Fe (III) 4-fluoro-N '- [(pyridine-4-yl) carbonyl] benzohydrazide complex compound have a maximum wavelength of 265.6 nm. The absorption of functional groups on the 540.0 cm-1 infra red wave spectrum.

 Keywords: synthesis, complex, Fe (III), benzohydrazide

 

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