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{"title":"热障涂层用机械合金化Ni22Cr11Al粉末的火花等离子烧结组织和力学性能","authors":"F. Omoniyi, P. Olubambi, R. Sadiku","doi":"10.4172/2169-0022.1000485","DOIUrl":null,"url":null,"abstract":"Thermal barrier coatings (TBCs) systems are used to protect hot sections of industrial gas turbine blades against high temperature corrosion and oxidation. Currently, MCrAlY powders up to 100 μm in diameter are used in the production of thermal barrier coatings by industrial gas turbine component manufacturers. It has been found that nanocrystalline MCrAlY layer provide better oxidation behaviour than currently used microstructure MCrAlY layer at elevated temperature. In the present study, nanocrystalline NI22Cr11Al composites was synthesized using high energy planetary ball milling for different periods of time, and the dense NI22Cr11Al alloy was fabricated by using spark plasma sintering process at different temperatures ranging from 1000°C to 1200°C. The resultant powder particles, bulk and dense samples were characterised using scanning electron microscope (SEM), X-ray diffraction analysis (XRD) and Micro Vickers hardness test. The results indicated that mechanical milling process produce morphology changes, particle size increase, crystallite size decrease down to nanometric level (40 nm) and formation of Nano dispersions in the process. *Corresponding author: Omoniyi FIS, College of Science, Engineering and Food Science, University College Cork Ireland, Tel: +353899801944; E-mail: folorunsoomoniyi@gmail.com Received September 07, 2018; Accepted September 19, 2018; Published September 29, 2018 Citation: Omoniyi FIS, Olubambi PA, Sadiku RE (2018) Microstructural and Mechanical Properties of Spark Plasma Sintering of Ni22Cr11Al Powders Synthesized by Mechanical Alloying for Thermal Barrier Coating. J Material Sci Eng 7: 485. doi: 10.4172/2169-0022.1000485 Copyright: © 2018 Omoniyi FIS, et al. This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.","PeriodicalId":16326,"journal":{"name":"Journal of Material Sciences & Engineering","volume":"18 1","pages":"1-8"},"PeriodicalIF":0.0000,"publicationDate":"2018-09-29","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Microstructural and Mechanical Properties of Spark Plasma Sintering of Ni22Cr11Al Powders Synthesized by Mechanical Alloying for Thermal Barrier Coating\",\"authors\":\"F. Omoniyi, P. Olubambi, R. Sadiku\",\"doi\":\"10.4172/2169-0022.1000485\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Thermal barrier coatings (TBCs) systems are used to protect hot sections of industrial gas turbine blades against high temperature corrosion and oxidation. Currently, MCrAlY powders up to 100 μm in diameter are used in the production of thermal barrier coatings by industrial gas turbine component manufacturers. It has been found that nanocrystalline MCrAlY layer provide better oxidation behaviour than currently used microstructure MCrAlY layer at elevated temperature. In the present study, nanocrystalline NI22Cr11Al composites was synthesized using high energy planetary ball milling for different periods of time, and the dense NI22Cr11Al alloy was fabricated by using spark plasma sintering process at different temperatures ranging from 1000°C to 1200°C. The resultant powder particles, bulk and dense samples were characterised using scanning electron microscope (SEM), X-ray diffraction analysis (XRD) and Micro Vickers hardness test. The results indicated that mechanical milling process produce morphology changes, particle size increase, crystallite size decrease down to nanometric level (40 nm) and formation of Nano dispersions in the process. *Corresponding author: Omoniyi FIS, College of Science, Engineering and Food Science, University College Cork Ireland, Tel: +353899801944; E-mail: folorunsoomoniyi@gmail.com Received September 07, 2018; Accepted September 19, 2018; Published September 29, 2018 Citation: Omoniyi FIS, Olubambi PA, Sadiku RE (2018) Microstructural and Mechanical Properties of Spark Plasma Sintering of Ni22Cr11Al Powders Synthesized by Mechanical Alloying for Thermal Barrier Coating. J Material Sci Eng 7: 485. doi: 10.4172/2169-0022.1000485 Copyright: © 2018 Omoniyi FIS, et al. 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Microstructural and Mechanical Properties of Spark Plasma Sintering of Ni22Cr11Al Powders Synthesized by Mechanical Alloying for Thermal Barrier Coating
Thermal barrier coatings (TBCs) systems are used to protect hot sections of industrial gas turbine blades against high temperature corrosion and oxidation. Currently, MCrAlY powders up to 100 μm in diameter are used in the production of thermal barrier coatings by industrial gas turbine component manufacturers. It has been found that nanocrystalline MCrAlY layer provide better oxidation behaviour than currently used microstructure MCrAlY layer at elevated temperature. In the present study, nanocrystalline NI22Cr11Al composites was synthesized using high energy planetary ball milling for different periods of time, and the dense NI22Cr11Al alloy was fabricated by using spark plasma sintering process at different temperatures ranging from 1000°C to 1200°C. The resultant powder particles, bulk and dense samples were characterised using scanning electron microscope (SEM), X-ray diffraction analysis (XRD) and Micro Vickers hardness test. The results indicated that mechanical milling process produce morphology changes, particle size increase, crystallite size decrease down to nanometric level (40 nm) and formation of Nano dispersions in the process. *Corresponding author: Omoniyi FIS, College of Science, Engineering and Food Science, University College Cork Ireland, Tel: +353899801944; E-mail: folorunsoomoniyi@gmail.com Received September 07, 2018; Accepted September 19, 2018; Published September 29, 2018 Citation: Omoniyi FIS, Olubambi PA, Sadiku RE (2018) Microstructural and Mechanical Properties of Spark Plasma Sintering of Ni22Cr11Al Powders Synthesized by Mechanical Alloying for Thermal Barrier Coating. J Material Sci Eng 7: 485. doi: 10.4172/2169-0022.1000485 Copyright: © 2018 Omoniyi FIS, et al. This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.