热障涂层用机械合金化Ni22Cr11Al粉末的火花等离子烧结组织和力学性能

F. Omoniyi, P. Olubambi, R. Sadiku
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摘要

热障涂层(tbc)系统用于保护工业燃气轮机叶片的热部分免受高温腐蚀和氧化。目前,直径达100 μm的MCrAlY粉末被工业燃气轮机部件制造商用于生产热障涂层。研究发现,纳米晶MCrAlY层在高温下比目前使用的微结构MCrAlY层具有更好的氧化性能。本研究采用高能行星球磨不同时间合成纳米晶NI22Cr11Al复合材料,并在1000℃~ 1200℃不同温度下采用火花等离子烧结工艺制备致密NI22Cr11Al合金。采用扫描电镜(SEM)、x射线衍射分析(XRD)和显微维氏硬度测试对所得粉末颗粒、体状和致密样品进行了表征。结果表明:机械铣削过程中形貌发生变化,晶粒尺寸增大,晶粒尺寸减小至纳米级(40 nm),并形成纳米分散体;*通讯作者:Omoniyi FIS,爱尔兰科克大学学院科学、工程和食品科学学院,电话:+353899801944;邮箱:folorunsoomoniyi@gmail.com 2018年9月07日收稿;2018年9月19日录用;引用本文:Omoniyi FIS, Olubambi PA, Sadiku RE(2018)火花等离子烧结机械合金化制备Ni22Cr11Al热障涂层粉末的显微组织和力学性能。[J] .材料科学与工程学报,7(5):483。doi: 10.4172/2169-0022.1000485版权所有:©2018 Omoniyi FIS等这是一篇根据知识共享署名许可协议发布的开放获取文章,该协议允许在任何媒体上不受限制地使用、分发和复制,前提是要注明原作者和来源。
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Microstructural and Mechanical Properties of Spark Plasma Sintering of Ni22Cr11Al Powders Synthesized by Mechanical Alloying for Thermal Barrier Coating
Thermal barrier coatings (TBCs) systems are used to protect hot sections of industrial gas turbine blades against high temperature corrosion and oxidation. Currently, MCrAlY powders up to 100 μm in diameter are used in the production of thermal barrier coatings by industrial gas turbine component manufacturers. It has been found that nanocrystalline MCrAlY layer provide better oxidation behaviour than currently used microstructure MCrAlY layer at elevated temperature. In the present study, nanocrystalline NI22Cr11Al composites was synthesized using high energy planetary ball milling for different periods of time, and the dense NI22Cr11Al alloy was fabricated by using spark plasma sintering process at different temperatures ranging from 1000°C to 1200°C. The resultant powder particles, bulk and dense samples were characterised using scanning electron microscope (SEM), X-ray diffraction analysis (XRD) and Micro Vickers hardness test. The results indicated that mechanical milling process produce morphology changes, particle size increase, crystallite size decrease down to nanometric level (40 nm) and formation of Nano dispersions in the process. *Corresponding author: Omoniyi FIS, College of Science, Engineering and Food Science, University College Cork Ireland, Tel: +353899801944; E-mail: folorunsoomoniyi@gmail.com Received September 07, 2018; Accepted September 19, 2018; Published September 29, 2018 Citation: Omoniyi FIS, Olubambi PA, Sadiku RE (2018) Microstructural and Mechanical Properties of Spark Plasma Sintering of Ni22Cr11Al Powders Synthesized by Mechanical Alloying for Thermal Barrier Coating. J Material Sci Eng 7: 485. doi: 10.4172/2169-0022.1000485 Copyright: © 2018 Omoniyi FIS, et al. This is an open-access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.
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