石墨烯晶格片碳纤维增强层压复合材料的制备、加工与表征

V. Jadhav, A. Kelkar
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摘要

本文介绍了石墨烯片增强无卷曲织物(NCF)复合层压板制造中的挑战及其对复合层压板层间强度的影响。在目前的工作中,层压板是用无卷曲的碳织物预浸料和50,120和240 μm厚的石墨烯片在中层制备的。双悬臂梁(DCB)测试按照ASTM 5528使用INSTRON机电测试系统完成。修正梁理论方法采用荷载、位移、试件尺寸和裂纹张开位移计算I型断裂韧性。石墨烯薄片很脆;在制造过程中,石墨烯与基体之间的结合很少,导致界面脆弱。为了克服这个问题,石墨烯片被转换成晶格结构。本研究中使用的点阵结构有水平网格、垂直网格和方形网格。采用I型断裂韧性评价了加和不加纳米工程增强层压板对板厚、网格模式的影响。用Axio Image立式显微镜比较DCB测试后背板的粘结情况。结果表明,采用点阵石墨烯结构制备的复合材料层压板具有较好的层间强度。
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Fabrication, Processing and Characterization of Carbon Fibre Reinforced Laminated Composite Embedded With Graphene Lattice Sheets
This manuscript introduces the challenges in the fabrication of graphene sheet reinforced non-crimp fabric (NCF) composite laminates and their influence on the interlaminar strength of the composite laminates. In the current work, the laminates were fabricated using non-crimp carbon fabric prepreg along with 50,120 and 240 μm thick graphene sheets at the mid-plane. Double Cantilever Beam (DCB) tests are done as per ASTM 5528 using INSTRON electromechanical testing system. Modified Beam Theory method used to compute Mode I fracture toughness, using load, displacement, specimen dimension, and crack opening displacement. The graphene sheets are brittle; little bonding between the graphene and matrix observed during the fabrication process results in a fragile interface. To overcome this problem, graphene sheets were converted into a lattice structure. The lattice structure used in the present research had horizontal, vertical, and square grids. Effects of sheet thickness, grid pattern were evaluated by Mode I fracture toughness, with and without nanoengineered enhanced laminates. Axio Image upright microscope used to compare the bonding at the midplane after the DCB test. The results indicate that the composite laminates fabricated using lattice graphene structure had better interlaminar strength than the laminates fabricated with straight graphene sheets.
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