气相色谱-质谱及傅里叶变换红外光谱分析Benth。豆荚甲醇提取物

Purendra Singh
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摘要

摘要本研究旨在阐明小檗(Albizia lebbeck, L.)甲醇提取物中存在的生物活性化合物。Benth。Pod采用气相色谱-质谱(GC-MS)和傅里叶变换红外光谱(FTIR)技术。鉴定化合物的GC-MS质谱与美国国家标准与技术研究所(NIST)数据库的质谱进行比较。结果证实甲醇提取物中存在五种化合物:五硅氧烷,1,1,3,3,5,5,7,7,9,9-十甲基-,七硅氧烷,十六甲基-,糖胆酸甲酯,3TMS衍生物,(5a)孕烷-3,20a-二醇,14a,18a-[4-甲基-3-氧-(1-氧-4-阿扎丁烷-1,4 -二基)]-,二乙酸酯,环十硅氧烷,二十甲基。这些生物活性化合物在植物中的存在为合欢的传统使用提供了一个平台。Benth。治疗各种疾病。FTIR光谱研究表明,豆荚提取物中存在C- f拉伸(1018.08)、C- O拉伸(1112.70)、(-C-H)弯曲、拉伸(1409.04)、(C=C)拉伸(1647.62)、(N-H)拉伸(2832.78)、(C-H)拉伸(2943.06)、(O-H)拉伸(3321.22)等官能团。
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Gas chromatography mass spectrometry and Fourier transform infrared spectral analyses of Albizia lebbeck (L.) Benth. pod methanol extract
This study was aimed at the elucidation of the bioactive compounds present in methanol extracts of Albizia lebbeck (L.) Benth. Pod using Gas chromatography–mass spectrometry (GC-MS) and Fourier transform infrared spectroscopic (FTIR) techniques. The GC-MS mass spectra of the identified compounds were compared with those of the National Institute of Standards and Technology (NIST) database library. The results confirmed the presence of  five compounds  including  Pentasiloxane, 1,1,3,3,5,5,7,7,9,9-decamethyl-, Heptasiloxane, hexadecamethyl-, Methyl glycocholate, 3TMS derivative, (5a)Pregnane-3,20a-diol, 14a,18a-[4-methyl-3-oxo-(1-oxa-4-azabutane-1,4 -diyl)]-, diacetate, Cyclodecasiloxane, eicosamethyl were found in methanol extracts.  The presence of these bioactive compounds in the plant offers a platform for the traditional use of Albizia lebbeck (L.) Benth. in treatment of various diseases. The FTIR spectroscopic studies revealed the presence of these functional groups: C-F stretch (1018.08 ),   C – O stretch (1112.70), (-C-H) Bending, stretch (1409.04), (C=C) stretch (1647.62), (N-H) stretch (2832.78), (C-H) stretch (2943.06), (O-H) (stretch, H- bonded) (3321.22) in the pod extracts.
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