医用钛电沉积超亲水性磷酸盐团块涂层的选择

D. C. Romonți, G. Anghel, G. Voicu
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引用次数: 0

摘要

为了在钛表面制备一层亲水性很强的磷酸盐团块涂层,对样品进行了抛光、刻蚀和超声处理后的电沉积方法。在不同的工作参数(时间和温度)下,在三个电极池中进行电沉积。电沉积后,所有样品在4000C下煅烧1小时,以提高结晶度和纯度。表征包括FT-IR、SEM、XRD、AFM和接触角测定,表明涂层具有斑块晶体和小针状HAP的粗糙涂层,具有良好的Ca/P比和超亲水性。高表面能表明良好的生物粘附性。
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Selecting super hydrophilic phosphate masses coatings electrodeposited on titanium for medical applications
In order to elaborate a very strong hydrophilic phosphate masses coating on titanium, an electrodeposition method was performed after polishing, etching and ultrasonication of samples. Electrodeposition took place in three electrodes cell at different working parameters (time and temperature). After electrodeposition all samples were calcinated for 1 hour at 4000C, in order to increase the crystalinitty and the purity. The coating characterization has included FT-IR SEM, XRD, AFM, and contact angle determinations and has indicated a rough coating with plaques crystals and small needles of HAP, good ratio Ca/P, and superhydrophilic character. The high surface energy denotes good bioadhesion.
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