基于优质碳化硅纳米纤维的纳米复合材料的初步研究

S. Bellucci, I. Sacco, F. Micciulla, A. Dąbrowska, A. Huczko, E. Caponetti, M. Floriano, A. Dinescu
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引用次数: 2

摘要

纳米复合材料由于其独特的性能(如高机械强度、耐化学性和耐热性)而成为当今最有前途的新材料。纳米复合材料基体与纳米结构填料混合。在这项研究中,碳化硅纳米纤维(NFSiC)及其束作为两种环氧树脂:EPIKOTE 828和EL 20的增强剂进行了测试。在两种情况下,分别使用PAP-4 (33 phr)和P-900 (40 phr)作为硬化剂。为两种类型的树脂和填料(NFSiC和NFSiC束)在0.1和5% wt之间制备了几个样品。测试了材料的机械和电气性能。采用一种简单、快速、低成本、高效的纳米材料合成新方法——自蔓延高温合成(SHS)获得了填料。采用扫描电镜(SEM)、透射电镜(TEM)对制备的纳米填料进行了分析。它们也被净化了。用扫描电镜和透射电镜对所制备的纳米复合材料进行了分析。
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Preliminary studies on nanocomposite based on high quality Silicon Carbide nanofibers
Nanocomposites are nowadays the most promising new materials due to their unique properties (such as high mechanical strength, chemical and thermal resistance). The nanocomposite matrix is blended with a nanostructured filler. In this study, Silicon Carbide nanofibers (NFSiC) and their bundles were tested as a reinforcement of two epoxy resins: EPIKOTE 828 and EL 20. PAP-4 (33 phr) and P-900 (40 phr) were used as hardeners in the two cases, respectively. Several samples were prepared in the range between 0.1 and 5 % wt for both types of resins and fillers (NFSiC and NFSiC bundles). Mechanical and electrical properties were tested. The fillers were obtained using a new simple, fast, low-cost and efficient method to synthesize nanomaterials: Self-propagating High-Temperature Synthesis (SHS). The produced nanofillers were analyzed by Scanning Electron Microscope (SEM), Trasmission Electron Microscope (TEM). They were purified, as well. The nanocomposites obtained using such nanofillers were assayed by SEM and TEM techniques.
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