二氧化锰纳米棒修饰网印电极电化学测定食品中苏丹红染料

IF 2.9 Q2 ELECTROCHEMISTRY Journal of Electrochemical Science and Engineering Pub Date : 2022-07-30 DOI:10.5599/jese.1415
S. A. Ahmadi, P. Mohammadzadeh Jahani
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引用次数: 2

摘要

制备了一种新型二氧化锰纳米棒修饰的丝网印刷电极,并将其用作测定苏丹酸的伏安传感器。采用场发射扫描电镜(FE-SEM)对二氧化锰纳米棒进行了表征。电化学测量采用循环伏安法(CV)、线性扫描伏安法(LSV)、差分脉冲伏安法(DPV)和计时伏安法(CA)。电极表面的二氧化锰纳米棒是苏丹氧化反应的优良催化剂。该修饰电极对苏丹红具有良好的电催化活性,响应时间短,小于10 s,检测限低,约为0.08µM,线性检测范围为0.25 ~ 300.0µM。
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MnO2 nanorods modified screen-printed electrode for the electrochemical determination of Sudan dye in food sample
A novel MnO2 nanorods modified screen-printed electrode was fabricated and used as a voltammetric sensor for Sudan determination. MnO2 nanorods were characterized using Field emission-scanning electron microscopy (FE-SEM). Electrochemical measurements were performed using cyclic voltammetry (CV), linear sweep voltammetry (LSV), differential pulse voltammetry (DPV), and chronoammperometry (CA). The MnO2 nanorods on the electrode surface act as an excellent catalyst for the Sudan oxidation reaction. Our modified electrode presents good electrocatalytic activity toward Sudan, a short response time of <10 s, a low detection limit of around 0.08 µM, and linear detection range from 0.25 to 300.0 µM.
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来源期刊
CiteScore
3.60
自引率
27.30%
发文量
90
审稿时长
6 weeks
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