丝胶蛋白作为生物模板用于银纳米颗粒的合成及表征

M. Shilpa, K. Harisha, S. Asha, N. Parushuram, R. Ranjana, Y. Sangappa
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引用次数: 4

摘要

本文介绍了利用蚕丝丝胶原位合成纳米银粒子(AgNPs)的方法。通过紫外可见光谱(UV-Vis)、x射线衍射(XRD)、透射电子显微镜(TEM)和动态光散射(DLS)实验证实了SS溶液中银纳米颗粒的形成。SS-AgNPs胶体的紫外可见吸收光谱在418 ~ 425 nm波长范围内显示出表面等离子体共振,证实了银纳米颗粒的形成。XRD扫描显示银的纳米晶相具有FCC晶体结构。TEM图像显示,制备的银纳米颗粒呈球形,边缘光滑,颗粒直径约为5 ~ 20nm。DLS结果表明,纳米颗粒的平均尺寸比TEM值略大。所有的结果都支持丝胶作为一个突出的生物模板还原银离子为银中性原子。本文介绍了利用蚕丝丝胶原位合成纳米银粒子(AgNPs)的方法。通过紫外可见光谱(UV-Vis)、x射线衍射(XRD)、透射电子显微镜(TEM)和动态光散射(DLS)实验证实了SS溶液中银纳米颗粒的形成。SS-AgNPs胶体的紫外可见吸收光谱在418 ~ 425 nm波长范围内显示出表面等离子体共振,证实了银纳米颗粒的形成。XRD扫描显示银的纳米晶相具有FCC晶体结构。TEM图像显示,制备的银纳米颗粒呈球形,边缘光滑,颗粒直径约为5 ~ 20nm。DLS结果表明,纳米颗粒的平均尺寸比TEM值略大。所有的结果都支持丝胶作为一个突出的生物模板还原银离子为银中性原子。
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Silk sericin a bio-template for the synthesis of silver nanoparticles and characterization
The research paper describes the in situ synthesis of silver nanoparticles (AgNPs) using Bombyxmorisilk sericin (SS). The formation of silver nanoparticles in the SS solution was confirmed by using UV-Visible spectroscopy (UV-Vis), X-ray diffraction measurements (XRD), transmission electron microscopy (TEM) and dynamic light scattering (DLS) experiments. The UV-Vis absorption spectra of the SS-AgNPs colloids showed surface Plasmon resonance in the wavelength range of 418-425 nm confirms the silver nanoparticles formation. The XRD scan revealed the nanocrystalline phase of silver with FCC crystal structure. The TEM images shown the formed silver nanoparticles are spherical in shape with smooth edges and diameter of the particles around 5-20 nm. The DLS results indicated the average size of the nanoparticles is slightly bigger in size compared with TEM values. All the results support the sericin as a prominent bio-template for reduction of silver ions to silver neutral atoms.The research paper describes the in situ synthesis of silver nanoparticles (AgNPs) using Bombyxmorisilk sericin (SS). The formation of silver nanoparticles in the SS solution was confirmed by using UV-Visible spectroscopy (UV-Vis), X-ray diffraction measurements (XRD), transmission electron microscopy (TEM) and dynamic light scattering (DLS) experiments. The UV-Vis absorption spectra of the SS-AgNPs colloids showed surface Plasmon resonance in the wavelength range of 418-425 nm confirms the silver nanoparticles formation. The XRD scan revealed the nanocrystalline phase of silver with FCC crystal structure. The TEM images shown the formed silver nanoparticles are spherical in shape with smooth edges and diameter of the particles around 5-20 nm. The DLS results indicated the average size of the nanoparticles is slightly bigger in size compared with TEM values. All the results support the sericin as a prominent bio-template for reduction of silver ions to silver neutral atoms.
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