微波辐照对虾壳废渣中壳聚糖提取的影响

Dwi Apriyanti, H. Susanto, N. Rokhati
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引用次数: 11

摘要

壳聚糖是一种无毒、可生物降解、生物相容性好的天然多糖,在保健、食品、农业和工业等领域具有广泛的应用价值。在甲壳素脱乙酰过程中,采用常规方法提取壳聚糖需要较长时间。壳聚糖的原料可以从虾壳废料中找到。壳聚糖的生产通常需要高温和大量的化学物质,耗时长,能耗大,对环境有不良影响。近年来,微波辐射作为一种非常规能源在化学反应中得到了广泛的应用。为了减少化学处理对环境污染的影响,本研究的目的是在微波辐照下处理壳聚糖。预期生产相同质量的壳聚糖比传统加热所需的化学物质更少。特别是,本研究将考察传统加热方法对壳聚糖的制备和添加化学物质、反应时间和操作温度以及壳聚糖脱乙酰程度的影响,并将结果与微波进行比较。本研究将在实验室研究规模上获得最佳结果后,进一步设计和制造虾壳废料制备壳聚糖的原型规模萃取器。从研究中我们可以得出结论,微波会加快反应时间。红外光谱也显示微波辐照后壳聚糖形成的官能团具有相同的结果。关键词:壳聚糖,虾壳,微波
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Influence of Microwave Irradiation on Extraction of Chitosan from Shrimp Shell Waste
Chitosan is natural polysaccharides which is nontoxic, biodegradable, and biocompatible and have many advantages in various kinds of fields including health, food, agriculture, and industry. Chitosan usually take long time to extract by conventional method for deacetylation process of chitin. Raw material for chitosan can be found in shrimp shell waste. Chitosan manufactures usually need high temperatures and chemicals in large quantities and it takes much time and consumes a lot of energy where will give bad effect to the environment. Recently microwave irradiation as nonconventional energy sources is widely used in chemical reactions. To reduce the impact of environmental pollution due to excessive use of chemical treatment, the objective of this work is processing chitosan under microwave irradiation. Expected production of chitosan with the same mass requires fewer chemicals than conventional heating. In particular, the study will examine the effect of making the chitosan and adding chemicals, reaction time and operating temperature and degree of deacetylation in chitosan with conventional heating methods that the results will be compared using a microwave. In this research will be developed to the design and fabrication of prototype scale extractor for manufacturing chitosan from shrimp shell waste after optimum results obtained from the research laboratory scale. From the research we can conclude that microwave will speed up reaction time. FTIR also showed functional group of chitosan formed from microwave irradiation have same results.  Keywords: chitosan, shrimp shells, microwave
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审稿时长
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