氧化锆-石墨陶瓷碳复合材料的生长、表征和比较

V. Kumari, S. Rani, Dharvendra Singh
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引用次数: 0

摘要

采用保守的固体烧结技术制备的ZrO2陶瓷碳复合材料的密度与任何市售的ZrO2一样接近。与较低的1200°C HTT样品相比,经过1400°C高温处理的样品的维氏硬度和模量相当高。从S1到S6对比发现,S6孔隙度最小,S1孔隙度最大。与陶瓷单体相比,其抗弯强度和模量有了显著提高。从x射线峰宽度测量的平均晶粒尺寸,x射线衍射图突出显示的信息来自晶格的更深层次。光学显微照片显示,除炭化过程中沥青泄漏引起的小颗粒外,样品均匀。其余的显微照片有助于发现颗粒大小以及沥青渗入体系的程度。
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Growth, Characterization and Comparison of Zirconia-Graphite Ceramic Carbon Composites
The density of ZrO2 ceramic carbon composites prepared by the conservative solid sintering technique is as close to any commercially available ZrO2. The Vicker's hardness as well as modulus of the sample with 1400°C high temperatures treated, is quite high compared to the lower 1200°C HTT samples. From S1 to S6 on comparison, it is found that porosity for S6 is minimum and maximum for S1. After comparing with ceramic monolith the flexural strength and modulus shows a remarkable improvement in its value. The average grain size measured from the width of the x-ray peaks, the information highlighted by x-ray diffractogram comes from a deeper level of the lattice. The optical micrograph shows the sample was uniform except for asperities arising due to leakage of pitch while carbonizing. The rest of the micrographs help in finding the grain size as well as the extent of infiltration of pitch into the system.
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