{"title":"ENKAPSULASI FRAKSI N-HEKSAN DAUN KESUM (Polygonum Minus Huds) TERSALUT Carboxymethylcellulose (CMC) DAN PATI DAN UJI AKTIVITAS ANTIOKSIDAN DENGAN TEKNIK FREEZE DRYING","authors":"F. Fitriani, M. A. Wibowo, A. Alimuddin","doi":"10.26418/indonesian.v2i1.36945","DOIUrl":null,"url":null,"abstract":"Kesum have a scientific name Polygonum Minus Huds is one of the endemic plants originating from West Borneo. Extracts of kesum leaf is easily damaged and the compounds contained therei are volatile. Therefore it is necessary to take measures to protect the extracts of kesum leaf. One effort that can be made to im exprove the stability of the compounds in the extract is by the process of encapsulation. This process needs to be done so that the leaf extract can last longer so it can be used for various purposes. Encapsulation aims to protect sensitive material components and reduce the degradation of the active compounds in the material. This study aims to determine the effect of mass of core materials on the efficiency of encapsulation and antioxidant activity and the effect of temperature on encapsulation. The results showed that the encapsulated with the mass of core material 10% gave the highest efficiency of 89.7%. The mass of the core material affects the encapsulation efficiency, the less the core material will provide a high value of encapsulation efficiency. Enkapsulates containing n-heksan fractions of 444.53 ppm have a lower value IC50, thus having better antioxidant activity properties. The stability of the encapsulated antioxidant activity performed at room temperature 25◦C at 10% n-hexane fraction yielded 88.36% ihibisi on day 1, 80.90% on day 3, 79.67% on day 6 and 78.04% on day 9. Activity the antioxidant encapsulant on the first day at room temperature 25◦C is better than the third, sixth and ninth days. SEM leaf extract analysis results have uneven spherical particles, no visible fracture or pore holes as large as encapsulation have round particles that are almost as large.","PeriodicalId":13554,"journal":{"name":"Indonesian Journal of Pure and Applied Chemistry","volume":null,"pages":null},"PeriodicalIF":0.0000,"publicationDate":"2019-04-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Indonesian Journal of Pure and Applied Chemistry","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.26418/indonesian.v2i1.36945","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
摘要
Kesum有一个学名Polygonum Minus Huds是一种源自西婆罗洲的特有植物。kesum叶提取物易被破坏,其所含化合物具有挥发性。因此,有必要采取措施保护kesum叶提取物。可以通过包封的方法来改善提取物中化合物的稳定性。这个过程需要完成,这样叶子提取物可以持续更长时间,这样它就可以用于各种目的。封装的目的是保护材料的敏感成分,减少材料中活性化合物的降解。本研究旨在确定芯材质量对包封效率和抗氧化活性的影响,以及温度对包封的影响。结果表明,芯材质量为10%时,封装效率最高,为89.7%。芯材的质量影响封装效率,芯材的质量越少,提供的封装效率值越高。含有444.53 ppm n-heksan组分的胶囊IC50值较低,因此具有较好的抗氧化活性。室温25℃,正己烷含量为10%时,包封抗氧化活性的稳定性为:第1天为88.36%,第3天为80.90%,第6天为79.67%,第9天为78.04%。抗氧化包封剂在室温25℃下第1天的活性优于第3天、第6天和第9天。SEM叶提取物分析结果有不均匀的球形颗粒,没有可见的断裂或与包封一样大的孔洞,有几乎与包封一样大的圆形颗粒。
ENKAPSULASI FRAKSI N-HEKSAN DAUN KESUM (Polygonum Minus Huds) TERSALUT Carboxymethylcellulose (CMC) DAN PATI DAN UJI AKTIVITAS ANTIOKSIDAN DENGAN TEKNIK FREEZE DRYING
Kesum have a scientific name Polygonum Minus Huds is one of the endemic plants originating from West Borneo. Extracts of kesum leaf is easily damaged and the compounds contained therei are volatile. Therefore it is necessary to take measures to protect the extracts of kesum leaf. One effort that can be made to im exprove the stability of the compounds in the extract is by the process of encapsulation. This process needs to be done so that the leaf extract can last longer so it can be used for various purposes. Encapsulation aims to protect sensitive material components and reduce the degradation of the active compounds in the material. This study aims to determine the effect of mass of core materials on the efficiency of encapsulation and antioxidant activity and the effect of temperature on encapsulation. The results showed that the encapsulated with the mass of core material 10% gave the highest efficiency of 89.7%. The mass of the core material affects the encapsulation efficiency, the less the core material will provide a high value of encapsulation efficiency. Enkapsulates containing n-heksan fractions of 444.53 ppm have a lower value IC50, thus having better antioxidant activity properties. The stability of the encapsulated antioxidant activity performed at room temperature 25◦C at 10% n-hexane fraction yielded 88.36% ihibisi on day 1, 80.90% on day 3, 79.67% on day 6 and 78.04% on day 9. Activity the antioxidant encapsulant on the first day at room temperature 25◦C is better than the third, sixth and ninth days. SEM leaf extract analysis results have uneven spherical particles, no visible fracture or pore holes as large as encapsulation have round particles that are almost as large.