改性西米淀粉生物膜的制备与表征

D. Sondari, F. Falah, Riska Suryaningrum, F. P. Sari, Athanasia Amanda Septefani, W. K. Restu, Y. Sampora
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引用次数: 5

摘要

研究了用改性西米淀粉制备生物膜以改善其机械和物理性能。以西米淀粉和改性西米为原料(乙酰化、氧化、交联和沉淀)制备生物膜并对其进行表征。采用乙醇为溶剂沉淀法、乙酸酐对西米淀粉进行乙酰化改性、过氧化氢氧化改性和醋酸钠交联改性等方法对西米淀粉进行了改性。生物膜由改性西米制成,使用浓度为1.0%重量的甘油,其中甘油作为增塑剂赋予淀粉膜的热塑性。然后将天然西米制成的生物膜与改性西米淀粉制成的生物膜进行了比较。测定了改性西米淀粉对生物膜的含水率、接触角值、伸长率、抗拉强度等力学性能的影响。利用傅里叶变换红外光谱(FTIR)分析了生物膜的化学结构,并用扫描电镜(SEM)观察了生物膜的形态。改性西米淀粉用于生物膜的最佳工艺条件是乙酰化。关键词:生物膜,西米,乙酰化,氧化,交联,SEM, FTIR
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Biofilm Based on Modified Sago Starch: Preparation and Characterization
Biofilms made from modified sago starch to improve the mechanical and physical properties have been studied.  This study aimed to prepare and characterize biofilms from sago starch and modified sago (acetylation, oxidation, cross-link and precipitation). Modified of sago starch was prepared by some methods: precipitation using ethanol as solvent, acetylation modified of sago starch using acetic anhydride, oxidation modification using hydrogen peroxide and cross-link modification using sodium acetate. Biofilms were made from modified sago using glycerol with a concentration of 1.0% weight, where glycerol acts as a plasticizer to impart the thermoplasticity of the starch film. Biofilm made from native sago was then compared to biofilm from modified sago starch. The effects of modified sago starch to the biofilm were measured on its moisture contents, contact angle value, mechanical properties such as elongation and tensile strength. The chemical structures were evaluated by Fourier-transform infrared spectroscopy (FTIR) and morphology of biofilm were measured by Scanning Electron Microscope (SEM). The optimum condition of modified sago starch used in biofilm in this study is by acetylation. The result show that modified acetylation of sago starch can improve the properties of biofilm Keywords: biofilms, sago, acetylation, oxidation, cross link, SEM, FTIR
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