软化学法合成纳米CdO粉体及其抑菌活性评价

S. Balamurugan , A.R. Balu , K. Usharani , M. Suganya , S. Anitha , D. Prabha , S. Ilangovan
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引用次数: 73

摘要

以醋酸镉为前驱盐,采用简单的软化学方法合成了CdO纳米粉体。采用XRD、SEM、EDX和TEM对合成的纳米粉体进行了表征。XRD分析表明,该材料具有(1 1 1)择优取向的多晶性质,SAED图也证实了这一点。EDX光谱证实了纳米粉末中Cd和O的存在。用琼脂孔扩散法对3种细菌和真菌进行了抑菌活性研究,从抑菌区观察到的抑菌活性证实了合成的纳米CdO粉体对病原菌具有有效的抑菌作用。
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Synthesis of CdO nanopowders by a simple soft chemical method and evaluation of their antimicrobial activities

CdO nanopowders were synthesized by a simple soft chemical method using cadmium acetate as the precursor salt. The as-synthesized nanopowders were characterized by XRD, SEM, EDX and TEM analysis. Polycrystalline nature with a (1 1 1) preferential orientation is revealed by the XRD analysis, which was confirmed from the SAED pattern. The presence of Cd and O in the nanopowders is confirmed from the EDX spectrum. The presence of peaks at 417, 499, 620 and 669 cm−1 observed in the FTIR spectrum corresponds to the bonding between Cd and O. Antimicrobial activities were performed against three bacteria and fungi strains by the agar well diffusion method, and from the observed zones of inhibition, it is confirmed that the as-synthesized CdO nanopowders act as an effective antimicrobial agent against pathogenic microorganisms.

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